ethyl vanillate

Base Information

• Chemical Name: ethyl vanillate
• CAS No.: 773134-71-7
• Molecular Formula: C₁₂H₁₆O₄
• Molecular Weight: 224.257
• Mol file: 773134-71-7.mol

Synonyms:ethyl vanillate

Chemical Property of ethyl vanillate

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of ethyl vanillate

There total 5 articles about ethyl vanillate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethanol (64-17-5) + vanillin (121-33-5,8014-42-4) → ethyl 2-ethoxyethanoate (817-95-8) + ethyl 3,3-diethoxypropanoate (10601-80-6) + ethyl vanillate (773134-71-7) + oxalic acid diethyl ester (95-92-1) + diethyl malonate (105-53-3) + diethyl Fumarate (623-91-6) + Ethyl diethoxyacetate (6065-82-3) + Diethyl maleate (141-05-9) + succinic acid diethyl ester (123-25-1)

Guidance literature:

With [methyl-3-(butyl-4-sulfonate) imidazolium]CuPW₁₂O₄₀; oxygen; at 159.84 ℃; for 5h; under 6000.6 Torr;

DOI:10.1016/j.chempr.2019.05.021

Reference yield:

ethanol (64-17-5) + 3-methoxy-4-hydroxybenzoic acid (121-34-6) → ethyl 2-ethoxyethanoate (817-95-8) + ethyl 3,3-diethoxypropanoate (10601-80-6) + ethyl vanillate (773134-71-7) + oxalic acid diethyl ester (95-92-1) + diethyl malonate (105-53-3) + diethyl Fumarate (623-91-6) + Ethyl diethoxyacetate (6065-82-3) + Diethyl maleate (141-05-9) + succinic acid diethyl ester (123-25-1)

Guidance literature:

With [methyl-3-(butyl-4-sulfonate) imidazolium]CuPW₁₂O₄₀; oxygen; at 159.84 ℃; for 5h; under 6000.6 Torr;

DOI:10.1016/j.chempr.2019.05.021

Reference yield:

ethanol (64-17-5) + vanillin (121-33-5,8014-42-4) → ethyl vanillate (773134-71-7) + diethyl Fumarate (623-91-6) + Ethyl diethoxyacetate (6065-82-3) + Diethyl maleate (141-05-9) + succinic acid diethyl ester (123-25-1)

Guidance literature:

With oxygen; O₄₀PW₁₂^(3-)*Cu⁽²⁺⁾*C₈H₁₅N₂O₃S⁽¹⁺⁾; at 170 ℃; for 5h; under 7500.75 Torr; Autoclave;

DOI:10.1039/d1gc03114g

upstream raw materials:

Diazoethan

3-methoxy-4-hydroxybenzoic acid

ethanol

vanillin

Downstream raw materials:

3',4',7-trihydroxyflavone