p-methoxybenzaldehyde 9-fluorenyl imine

Base Information

• Chemical Name: p-methoxybenzaldehyde 9-fluorenyl imine
• CAS No.: 118133-90-7
• Molecular Formula: C₂₁H₁₇NO
• Molecular Weight: 299.372

Synonyms:p-methoxybenzaldehyde 9-fluorenyl imine

Chemical Property of p-methoxybenzaldehyde 9-fluorenyl imine

Chemical Property:

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Technology Process of p-methoxybenzaldehyde 9-fluorenyl imine

There total 4 articles about p-methoxybenzaldehyde 9-fluorenyl imine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

9H-fluoren-9-amine hydrochloride (5978-75-6) + 4-methoxy-benzaldehyde (123-11-5) → p-methoxybenzaldehyde 9-fluorenyl imine (118133-90-7)

Guidance literature:

With sodium; In methanol; for 9h;

DOI:10.1016/S0040-4020(01)87794-2

Reference yield: 91.0%

9H-fluoren-9-amine hydrochloride (5978-75-6) + 4-methoxy-benzaldehyde (123-11-5) → N-(4-methoxybenzylidene)-9H-fluoren-9-amine (118133-90-7)

Guidance literature:

DOI:10.1016/S0040-4020(01)80037-5

Reference yield: 72.0%

9-aminofluorene (525-03-1) + 4-methoxy-benzaldehyde (123-11-5) → N-(4-methoxybenzylidene)-9H-fluoren-9-amine (118133-90-7)

Guidance literature:

In toluene; at 20 ℃; for 1h; Molecular sieve;

DOI:10.1021/acs.orglett.6b02465

upstream raw materials:

9H-fluoren-9-amine hydrochloride

4-methoxy-benzaldehyde

9-aminofluorene

Downstream raw materials:

9-fluorenone

4-methoxyphenylacetamide

N-benzyl-4-methoxybenzamide

2,2-spiro(9',9'-fluorenyl)-4-(4'-methoxyphenyl)-7-phenyl-6,8-dioxo-3,7-diazabicyclo<3.3.0>octane

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