[Ir(H)2(P(i-Pr)2Ph)3]tetrakis[3,5-bis(trifluoromethyl)phenyl]borate

Base Information

Chemical Name:[Ir(H)2(P(i-Pr)2Ph)3]tetrakis[3,5-bis(trifluoromethyl)phenyl]borate
CAS No.:219800-72-3
Molecular Formula:C₃₂H₁₂BF₂₄*C₃₆H₅₉IrP₃
Molecular Weight:1640.23
Hs Code.:

Synonyms:[Ir(H)2(P(i-Pr)2Ph)3]tetrakis[3,5-bis(trifluoromethyl)phenyl]borate

Suppliers and Price of [Ir(H)2(P(i-Pr)2Ph)3]tetrakis[3,5-bis(trifluoromethyl)phenyl]borate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [Ir(H)2(P(i-Pr)2Ph)3]tetrakis[3,5-bis(trifluoromethyl)phenyl]borate

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Technology Process of [Ir(H)2(P(i-Pr)2Ph)3]tetrakis[3,5-bis(trifluoromethyl)phenyl]borate

There total 1 articles about [Ir(H)2(P(i-Pr)2Ph)3]tetrakis[3,5-bis(trifluoromethyl)phenyl]borate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: diμ-chlorotetrakis(η2-cyclooctene)diiridium(I)

: 1333-74-0
hydrogen

: 79060-88-1
sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate

: 6372-43-6
diisopropylphenylphosphane

: 219800-72-3
[Ir(H)2(P(i-Pr)2Ph)3]tetrakis[3,5-bis(trifluoromethyl)phenyl]borate

Guidance literature:: In fluorobenzene; benzene; Ar-atmosphere; addn. of soln. of phosphine (6 equiv.) to suspn. of Ir-complex (C6H6), bubbling H2 (20 min, room temp.), evapn., dissoln. (C6H5F), addn. of borate, stirring (2 h, room temp.); concn., filtration, evapn. (in vac.), suspending in toluene, heating (60°C), cooling (crystn.), collection, washing (toluene);
DOI:10.1021/ja981727e