2,2-Dimethyl-propionic acid 3-trimethylsilanyloxy-cyclohex-2-enylmethyl ester

Base Information

Chemical Name:2,2-Dimethyl-propionic acid 3-trimethylsilanyloxy-cyclohex-2-enylmethyl ester
CAS No.:1026252-95-8
Molecular Formula:C₁₅H₂₈O₃Si
Molecular Weight:284.471
Hs Code.:

Synonyms:2,2-Dimethyl-propionic acid 3-trimethylsilanyloxy-cyclohex-2-enylmethyl ester

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Chemical Property of 2,2-Dimethyl-propionic acid 3-trimethylsilanyloxy-cyclohex-2-enylmethyl ester

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Technology Process of 2,2-Dimethyl-propionic acid 3-trimethylsilanyloxy-cyclohex-2-enylmethyl ester

There total 3 articles about 2,2-Dimethyl-propionic acid 3-trimethylsilanyloxy-cyclohex-2-enylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18997-19-8
Chloromethyl pivalate

: 1026252-95-8
2,2-Dimethyl-propionic acid 3-trimethylsilanyloxy-cyclohex-2-enylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / NaI / acetone / 2.5 h / 25 °C

2: 1) Zn-dust, 2) CuCN, LiCl / 1) THF, 12 deg C, 2) 0 deg C, 5 min, 3) -78 deg C to -20 deg C, 8 h, 4) 0 deg C, 6 h

With sodium iodide; lithium chloride; zinc; In acetone;
DOI:10.1021/jo00055a010

Reference yield:

: 75-77-4
chloro-trimethyl-silane

: 930-68-7
cyclohexenone

: 53064-79-2
iodomethyl pivaloate

: 1026252-95-8
2,2-Dimethyl-propionic acid 3-trimethylsilanyloxy-cyclohex-2-enylmethyl ester

Guidance literature:: With lithium chloride; zinc; Yield given. Multistep reaction; 1) THF, 12 deg C, 2) 0 deg C, 5 min, 3) -78 deg C to -20 deg C, 8 h, 4) 0 deg C, 6 h;
DOI:10.1021/jo00055a010

Reference yield:

: 75-77-4
chloro-trimethyl-silane

: 930-68-7
cyclohexenone

: C₆H₁₁IO₂Zn

: 1026252-95-8
2,2-Dimethyl-propionic acid 3-trimethylsilanyloxy-cyclohex-2-enylmethyl ester

Guidance literature:: With 1.) CuCN*LiCl; Multistep reaction; 1.) THF, -30 deg C, 5 min, 2.) THF, from -78 to 25 deg C, 12 h;
DOI:10.1021/jo00283a006