(1S,3R)-3-(4-bromophenyl)-N-[(1R)-1-(naphthalen-1-yl)ethyl]cyclopentanamine

Base Information

Chemical Name:(1S,3R)-3-(4-bromophenyl)-N-[(1R)-1-(naphthalen-1-yl)ethyl]cyclopentanamine
CAS No.:1211472-82-0
Molecular Formula:C₂₃H₂₄BrN
Molecular Weight:394.354
Hs Code.:

Synonyms:(1S,3R)-3-(4-bromophenyl)-N-[(1R)-1-(naphthalen-1-yl)ethyl]cyclopentanamine

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Chemical Property of (1S,3R)-3-(4-bromophenyl)-N-[(1R)-1-(naphthalen-1-yl)ethyl]cyclopentanamine

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Technology Process of (1S,3R)-3-(4-bromophenyl)-N-[(1R)-1-(naphthalen-1-yl)ethyl]cyclopentanamine

There total 3 articles about (1S,3R)-3-(4-bromophenyl)-N-[(1R)-1-(naphthalen-1-yl)ethyl]cyclopentanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 160678-57-9
(R)-3-(4-bromophenyl)cyclopentan-1-one

: 3886-70-2
(R)-1-(1-Naphthyl)ethylamine

: 1211472-82-0
(1S,3R)-3-(4-bromophenyl)-N-[(1R)-1-(naphthalen-1-yl)ethyl]cyclopentanamine

Guidance literature:: (R)-3-(4-bromophenyl)cyclopentan-1-one; (R)-1-(1-Naphthyl)ethylamine; With sodium cyanoborohydride; acetic acid; In methanol; at 20 ℃; Inert atmosphere;

With sodium hydrogencarbonate; In methanol; water;

Reference yield:

: 5467-74-3
4-Bromophenylboronic acid

: 1211472-82-0
(1S,3R)-3-(4-bromophenyl)-N-[(1R)-1-(naphthalen-1-yl)ethyl]cyclopentanamine

Guidance literature:: Multi-step reaction with 2 steps

1: bis(ethylene)rhodium acetylacetonate; (R)-2,2'-bis(diphenylphosphanyl)-1,1'-binaphthyl / 1,4-dioxane; water / 3 h / Inert atmosphere; Reflux

2: sodium cyanoborohydride; acetic acid / methanol / 20 °C / Inert atmosphere

With sodium cyanoborohydride; acetic acid; bis(ethylene)rhodium acetylacetonate; (R)-2,2'-bis(diphenylphosphanyl)-1,1'-binaphthyl; In 1,4-dioxane; methanol; water;

Reference yield:

: 930-30-3
cyclopent-2-enone

: 1211472-82-0
(1S,3R)-3-(4-bromophenyl)-N-[(1R)-1-(naphthalen-1-yl)ethyl]cyclopentanamine

Guidance literature:: Multi-step reaction with 2 steps

1: bis(ethylene)rhodium acetylacetonate; (R)-2,2'-bis(diphenylphosphanyl)-1,1'-binaphthyl / 1,4-dioxane; water / 3 h / Inert atmosphere; Reflux

2: sodium cyanoborohydride; acetic acid / methanol / 20 °C / Inert atmosphere

With sodium cyanoborohydride; acetic acid; bis(ethylene)rhodium acetylacetonate; (R)-2,2'-bis(diphenylphosphanyl)-1,1'-binaphthyl; In 1,4-dioxane; methanol; water;