cis-N'-[2-(1H-indol-3-yl)ethyl]-N,N-dimethyl-1-phenylcyclohexane-1,4-diamine

Base Information

Chemical Name:cis-N'-[2-(1H-indol-3-yl)ethyl]-N,N-dimethyl-1-phenylcyclohexane-1,4-diamine
CAS No.:475097-56-4
Molecular Formula:C₂₄H₃₁N₃
Molecular Weight:361.53
Hs Code.:

Synonyms:cis-N'-[2-(1H-indol-3-yl)ethyl]-N,N-dimethyl-1-phenylcyclohexane-1,4-diamine

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Chemical Property of cis-N'-[2-(1H-indol-3-yl)ethyl]-N,N-dimethyl-1-phenylcyclohexane-1,4-diamine

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Technology Process of cis-N'-[2-(1H-indol-3-yl)ethyl]-N,N-dimethyl-1-phenylcyclohexane-1,4-diamine

There total 4 articles about cis-N'-[2-(1H-indol-3-yl)ethyl]-N,N-dimethyl-1-phenylcyclohexane-1,4-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4746-97-8
cyclohexanedione monoethylene ketal

: 475097-56-4
cis-N'-[2-(1H-indol-3-yl)ethyl]-N,N-dimethyl-1-phenylcyclohexane-1,4-diamine

Guidance literature:: Multi-step reaction with 4 steps

1.1: methanol; water

2.1: tetrahydrofuran / 0 - 20 °C

2.2: 0 - 20 °C

3.1: hydrogenchloride / water

4.1: acetic acid; sodium tris(acetoxy)borohydride / tetrahydrofuran; 1,2-dichloro-ethane / 96 h / Inert atmosphere

With hydrogenchloride; sodium tris(acetoxy)borohydride; acetic acid; In tetrahydrofuran; methanol; water; 1,2-dichloro-ethane; 1.1: |Strecker Aminoacid Synthesis / 2.1: |Bruylants Amination;
DOI:10.1021/ml500116x

Reference yield:

: 77253-85-1
dimethyl-(8-phenyl-1,4-dioxaspiro[4.5]decan-8-yl)amine

: 475097-56-4
cis-N'-[2-(1H-indol-3-yl)ethyl]-N,N-dimethyl-1-phenylcyclohexane-1,4-diamine

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / water

2: acetic acid; sodium tris(acetoxy)borohydride / tetrahydrofuran; 1,2-dichloro-ethane / 96 h / Inert atmosphere

With hydrogenchloride; sodium tris(acetoxy)borohydride; acetic acid; In tetrahydrofuran; water; 1,2-dichloro-ethane;
DOI:10.1021/ml500116x

Reference yield:

: 100-59-4
phenylmagnesium chloride

: 475097-56-4
cis-N'-[2-(1H-indol-3-yl)ethyl]-N,N-dimethyl-1-phenylcyclohexane-1,4-diamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrahydrofuran / 0 - 20 °C

1.2: 0 - 20 °C

2.1: hydrogenchloride / water

3.1: acetic acid; sodium tris(acetoxy)borohydride / tetrahydrofuran; 1,2-dichloro-ethane / 96 h / Inert atmosphere

With hydrogenchloride; sodium tris(acetoxy)borohydride; acetic acid; In tetrahydrofuran; water; 1,2-dichloro-ethane; 1.1: |Bruylants Amination;
DOI:10.1021/ml500116x