1-(4-chlorophenyl)-4-(5-(4-chlorophenyl)-2-(4-fluorophenyl)-1H-pyrrol-3-yl)-3-p-tolyl-1H-pyrazole

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Chemical Name:1-(4-chlorophenyl)-4-(5-(4-chlorophenyl)-2-(4-fluorophenyl)-1H-pyrrol-3-yl)-3-p-tolyl-1H-pyrazole
CAS No.:1443022-01-2
Molecular Formula:C₃₂H₂₂Cl₂FN₃
Molecular Weight:538.451
Hs Code.:

Synonyms:1-(4-chlorophenyl)-4-(5-(4-chlorophenyl)-2-(4-fluorophenyl)-1H-pyrrol-3-yl)-3-p-tolyl-1H-pyrazole

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Chemical Property of 1-(4-chlorophenyl)-4-(5-(4-chlorophenyl)-2-(4-fluorophenyl)-1H-pyrrol-3-yl)-3-p-tolyl-1H-pyrazole

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Technology Process of 1-(4-chlorophenyl)-4-(5-(4-chlorophenyl)-2-(4-fluorophenyl)-1H-pyrrol-3-yl)-3-p-tolyl-1H-pyrazole

There total 6 articles about 1-(4-chlorophenyl)-4-(5-(4-chlorophenyl)-2-(4-fluorophenyl)-1H-pyrrol-3-yl)-3-p-tolyl-1H-pyrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1443021-93-9
4-(4-chlorophenyl)-2-(1-(4-chlorophenyl)-3-p-tolyl-1H-pyrazol-4-yl)-1-(4-fluorophenyl)butane-1,4-dione

: 1443022-01-2
1-(4-chlorophenyl)-4-(5-(4-chlorophenyl)-2-(4-fluorophenyl)-1H-pyrrol-3-yl)-3-p-tolyl-1H-pyrazole

Guidance literature:: With ammonium acetate; acetic acid; at 110 ℃; for 20h;
DOI:10.1016/j.ejmech.2013.03.005

Reference yield:

: 1073-70-7
4-chlorophenylhydrazine hydrochloride

: 1443022-01-2
1-(4-chlorophenyl)-4-(5-(4-chlorophenyl)-2-(4-fluorophenyl)-1H-pyrrol-3-yl)-3-p-tolyl-1H-pyrazole

Guidance literature:: Multi-step reaction with 5 steps

1: acetic acid / ethanol / 24 h / 20 °C

2: trichlorophosphate / 5 h / 0 - 80 °C

3: sodium hydroxide / ethanol; water / 24 h / 20 °C

4: potassium cyanide / N,N-dimethyl-formamide / 4 h / 30 - 35 °C

5: acetic acid; ammonium acetate / 20 h / 110 °C

With potassium cyanide; ammonium acetate; acetic acid; sodium hydroxide; trichlorophosphate; In ethanol; water; N,N-dimethyl-formamide; 3: |Claisen-Schmidt Condensation / 5: |Paal-Knorr Pyrrole Synthesis;
DOI:10.1016/j.ejmech.2013.03.005

Reference yield:

: 386272-18-0
1-(4-chlorophenyl)-2-(1-p-tolylethylidene)hydrazine

: 1443022-01-2
1-(4-chlorophenyl)-4-(5-(4-chlorophenyl)-2-(4-fluorophenyl)-1H-pyrrol-3-yl)-3-p-tolyl-1H-pyrazole

Guidance literature:: Multi-step reaction with 4 steps

1: trichlorophosphate / 5 h / 0 - 80 °C

2: sodium hydroxide / ethanol; water / 24 h / 20 °C

3: potassium cyanide / N,N-dimethyl-formamide / 4 h / 30 - 35 °C

4: acetic acid; ammonium acetate / 20 h / 110 °C

With potassium cyanide; ammonium acetate; acetic acid; sodium hydroxide; trichlorophosphate; In ethanol; water; N,N-dimethyl-formamide; 2: |Claisen-Schmidt Condensation / 4: |Paal-Knorr Pyrrole Synthesis;
DOI:10.1016/j.ejmech.2013.03.005