(E)-3-(4-cyanophenyl)-2-methylpropenoate

Base Information

Chemical Name:(E)-3-(4-cyanophenyl)-2-methylpropenoate
CAS No.:58793-84-3
Molecular Formula:C₁₂H₁₁NO₂
Molecular Weight:201.225
Hs Code.:

Synonyms:(E)-3-(4-cyanophenyl)-2-methylpropenoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-3-(4-cyanophenyl)-2-methylpropenoate

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Technology Process of (E)-3-(4-cyanophenyl)-2-methylpropenoate

There total 4 articles about (E)-3-(4-cyanophenyl)-2-methylpropenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 623-00-7
4-bromobenzenecarbonitrile

: 80-62-6,114512-63-9,143476-91-9,25188-98-1,9011-14-7
methacrylic acid methyl ester

: 58793-84-3
(E)-3-(4-cyanophenyl)-2-methylpropenoate

Guidance literature:: With [CH₃PPh₃]₂[Pd₂Br₂Cl₄]; sodium hydrogencarbonate; In N,N-dimethyl-formamide; at 140 ℃; for 0.75h;
DOI:10.1055/s-0032-1317963

Reference yield:

: 5445-17-0
Methyl 2-bromopropionate

: 105-07-7
4-cyanobenzaldehyde

: 58793-84-3
(E)-3-(4-cyanophenyl)-2-methylpropenoate

: C₁₂H₁₁NO₂

Guidance literature:: With 1-phenylphospholane-1-oxide; 1,3-diphenyl-disiloxane; N-ethyl-N,N-diisopropylamine; In ethyl acetate; at 23 ℃; for 46h; Overall yield = 54 percent; Overall yield = 27.1 mg;
DOI:10.1055/s-0040-1707345

Reference yield:

: 623-00-7
4-bromobenzenecarbonitrile

: 80-62-6,114512-63-9,143476-91-9,25188-98-1,9011-14-7
methacrylic acid methyl ester

: 58793-84-3
(E)-3-(4-cyanophenyl)-2-methylpropenoate

: 58793-85-4
methyl 2-(4-cyanobenzyl)acrylate

Guidance literature:: With potassium carbonate; bis(η3-allyl-μ-chloropalladium(II)); (1RS,2RS,3SR,4SR)-1,2,3,4-tetrakis((diphenylphosphanyl)methyl)cyclopentane; In N,N-dimethyl-formamide; at 130 ℃; for 20h;
DOI:10.1016/j.tetlet.2003.09.092