(E)-1-<(p-methoxyphenyl)sulfonyl>-2-methyl-3-(N-methylformimidoyl)indole

Base Information

Chemical Name:(E)-1-<(p-methoxyphenyl)sulfonyl>-2-methyl-3-(N-methylformimidoyl)indole
CAS No.:85923-53-1
Molecular Formula:C₁₈H₁₈N₂O₃S
Molecular Weight:342.419
Hs Code.:

Synonyms:(E)-1-<(p-methoxyphenyl)sulfonyl>-2-methyl-3-(N-methylformimidoyl)indole

Suppliers and Price of (E)-1-<(p-methoxyphenyl)sulfonyl>-2-methyl-3-(N-methylformimidoyl)indole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-1-<(p-methoxyphenyl)sulfonyl>-2-methyl-3-(N-methylformimidoyl)indole

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Technology Process of (E)-1-<(p-methoxyphenyl)sulfonyl>-2-methyl-3-(N-methylformimidoyl)indole

There total 4 articles about (E)-1-<(p-methoxyphenyl)sulfonyl>-2-methyl-3-(N-methylformimidoyl)indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 80664-26-2
N-<(4-methoxyphenyl)sulfonyl>-2-methylindole-3-carboxaldehyde

: 74-89-5
methylamine

: 85923-53-1
(E)-1-<(p-methoxyphenyl)sulfonyl>-2-methyl-3-(N-methylformimidoyl)indole

Guidance literature:: In ethanol; at 25 ℃; for 18h;
DOI:10.1021/ja00262a005

Reference yield:

: 5416-80-8
2-methyl-1H-indole-3-carbaldehyde

: 85923-53-1
(E)-1-<(p-methoxyphenyl)sulfonyl>-2-methyl-3-(N-methylformimidoyl)indole

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) sodium hydride, 2.) imidazole / 1.) glyme, 20 deg C, 1.5 h, reflux, 15 min, 2.) 20 deg C, 15 h

2: CH₂Cl₂ / 15 h / 4 Angstroem molecular sieves

With 1H-imidazole; sodium hydride; In dichloromethane;
DOI:10.1021/ja00352a037

Reference yield:

: 98-68-0
4-methoxy-phenyl-sulphonyl chloride

: 85923-53-1
(E)-1-<(p-methoxyphenyl)sulfonyl>-2-methyl-3-(N-methylformimidoyl)indole

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) sodium hydride, 2.) imidazole / 1.) glyme, 20 deg C, 1.5 h, reflux, 15 min, 2.) 20 deg C, 15 h

2: CH₂Cl₂ / 15 h / 4 Angstroem molecular sieves

With 1H-imidazole; sodium hydride; In dichloromethane;
DOI:10.1021/ja00352a037