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ethyl-5-(2,4-dibenzyloxy-5-isopropylphenyl)-4-iodoisoxazole-3-carboxylate

Base Information Edit
  • Chemical Name:ethyl-5-(2,4-dibenzyloxy-5-isopropylphenyl)-4-iodoisoxazole-3-carboxylate
  • CAS No.:1133784-43-6
  • Molecular Formula:C29H28INO5
  • Molecular Weight:597.45
  • Hs Code.:
  • Mol file:1133784-43-6.mol
ethyl-5-(2,4-dibenzyloxy-5-isopropylphenyl)-4-iodoisoxazole-3-carboxylate

Synonyms:ethyl-5-(2,4-dibenzyloxy-5-isopropylphenyl)-4-iodoisoxazole-3-carboxylate

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The product has achieved commercial mass production*data from LookChem market partment
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Chemical Property of ethyl-5-(2,4-dibenzyloxy-5-isopropylphenyl)-4-iodoisoxazole-3-carboxylate Edit
Chemical Property:
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Technology Process of ethyl-5-(2,4-dibenzyloxy-5-isopropylphenyl)-4-iodoisoxazole-3-carboxylate

There total 8 articles about ethyl-5-(2,4-dibenzyloxy-5-isopropylphenyl)-4-iodoisoxazole-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With N-iodo-succinimide; ammonium cerium (IV) nitrate; In acetonitrile; at 20 ℃;
Guidance literature:
Multi-step reaction with 8 steps
1.1: potassium carbonate / acetonitrile / Reflux
2.1: potassium tert-butylate / tetrahydrofuran / 0 °C
2.2: 0 - 20 °C
3.1: palladium 10% on activated carbon; hydrogen / acetic acid; ethanol / 48 h / 20 °C / 7600.51 Torr
4.1: boron trifluoride diethyl etherate
5.1: potassium carbonate / acetonitrile / 20 °C
6.1: sodium ethanolate / ethanol / 20 °C
6.2: 20 °C
7.1: hydroxylamine hydrochloride / ethanol / 20 °C
8.1: N-iodo-succinimide; ammonium cerium (IV) nitrate / acetonitrile / 80 °C
With N-iodo-succinimide; ammonium cerium (IV) nitrate; palladium 10% on activated carbon; boron trifluoride diethyl etherate; hydroxylamine hydrochloride; potassium tert-butylate; hydrogen; sodium ethanolate; potassium carbonate; In tetrahydrofuran; ethanol; acetic acid; acetonitrile; 2.2: |Wittig Olefination / 4.1: |Friedel-Crafts Acylation;
DOI:10.1016/j.bmcl.2015.06.009
Guidance literature:
Multi-step reaction with 6 steps
1.1: palladium 10% on activated carbon; hydrogen / acetic acid; ethanol / 48 h / 20 °C / 7600.51 Torr
2.1: boron trifluoride diethyl etherate
3.1: potassium carbonate / acetonitrile / 20 °C
4.1: sodium ethanolate / ethanol / 20 °C
4.2: 20 °C
5.1: hydroxylamine hydrochloride / ethanol / 20 °C
6.1: N-iodo-succinimide; ammonium cerium (IV) nitrate / acetonitrile / 80 °C
With N-iodo-succinimide; ammonium cerium (IV) nitrate; palladium 10% on activated carbon; boron trifluoride diethyl etherate; hydroxylamine hydrochloride; hydrogen; sodium ethanolate; potassium carbonate; In ethanol; acetic acid; acetonitrile; 2.1: |Friedel-Crafts Acylation;
DOI:10.1016/j.bmcl.2015.06.009
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