(2S,3R,4R,5S,6R)-2-(2-(2-(1H-1,2,4-triazol-1-yl)ethoxy)-4-chloro-5-((5-(furan-2-yl)thiazol-2-yl)methyl)phenyl)-6-(hydroxymethyl)-tetrahydro-2H-pyran-3,4,5-triol

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Chemical Name:(2S,3R,4R,5S,6R)-2-(2-(2-(1H-1,2,4-triazol-1-yl)ethoxy)-4-chloro-5-((5-(furan-2-yl)thiazol-2-yl)methyl)phenyl)-6-(hydroxymethyl)-tetrahydro-2H-pyran-3,4,5-triol
CAS No.:1313513-35-7
Molecular Formula:C₂₄H₂₅ClN₄O₇S
Molecular Weight:549.004
Hs Code.:

Synonyms:(2S,3R,4R,5S,6R)-2-(2-(2-(1H-1,2,4-triazol-1-yl)ethoxy)-4-chloro-5-((5-(furan-2-yl)thiazol-2-yl)methyl)phenyl)-6-(hydroxymethyl)-tetrahydro-2H-pyran-3,4,5-triol

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Chemical Property of (2S,3R,4R,5S,6R)-2-(2-(2-(1H-1,2,4-triazol-1-yl)ethoxy)-4-chloro-5-((5-(furan-2-yl)thiazol-2-yl)methyl)phenyl)-6-(hydroxymethyl)-tetrahydro-2H-pyran-3,4,5-triol

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Technology Process of (2S,3R,4R,5S,6R)-2-(2-(2-(1H-1,2,4-triazol-1-yl)ethoxy)-4-chloro-5-((5-(furan-2-yl)thiazol-2-yl)methyl)phenyl)-6-(hydroxymethyl)-tetrahydro-2H-pyran-3,4,5-triol

There total 3 articles about (2S,3R,4R,5S,6R)-2-(2-(2-(1H-1,2,4-triazol-1-yl)ethoxy)-4-chloro-5-((5-(furan-2-yl)thiazol-2-yl)methyl)phenyl)-6-(hydroxymethyl)-tetrahydro-2H-pyran-3,4,5-triol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 1313513-28-8
(2S,3R,4R,5S,6R)-2-(4-chloro-5-((5-(furan-2-yl)thiazol-2-yl)methyl)-2-hydroxyphenyl)-6-(hydroxymethyl)-tetrahydro-2H-pyran-3,4,5-triol

: 41253-21-8
sodium triazole

: 106-93-4
ethylene dibromide

: 1313513-35-7
(2S,3R,4R,5S,6R)-2-(2-(2-(1H-1,2,4-triazol-1-yl)ethoxy)-4-chloro-5-((5-(furan-2-yl)thiazol-2-yl)methyl)phenyl)-6-(hydroxymethyl)-tetrahydro-2H-pyran-3,4,5-triol

Guidance literature:: (2S,3R,4R,5S,6R)-2-(4-chloro-5-((5-(furan-2-yl)thiazol-2-yl)methyl)-2-hydroxyphenyl)-6-(hydroxymethyl)-tetrahydro-2H-pyran-3,4,5-triol; ethylene dibromide; With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 60h; Inert atmosphere;

sodium triazole; In N,N-dimethyl-formamide; at 20 ℃; for 15h; Inert atmosphere;
DOI:10.1016/j.ejmech.2011.03.052

Reference yield:

: 1352714-18-1
C₂₂H₂₃BrClNO₇S

: 41253-21-8
sodium triazole

: 1313513-35-7
(2S,3R,4R,5S,6R)-2-(2-(2-(1H-1,2,4-triazol-1-yl)ethoxy)-4-chloro-5-((5-(furan-2-yl)thiazol-2-yl)methyl)phenyl)-6-(hydroxymethyl)-tetrahydro-2H-pyran-3,4,5-triol

Guidance literature:: In N,N-dimethyl-formamide; at 20 ℃; for 15h; Inert atmosphere;

Reference yield:

: 1313513-28-8
(2S,3R,4R,5S,6R)-2-(4-chloro-5-((5-(furan-2-yl)thiazol-2-yl)methyl)-2-hydroxyphenyl)-6-(hydroxymethyl)-tetrahydro-2H-pyran-3,4,5-triol

: 1313513-35-7
(2S,3R,4R,5S,6R)-2-(2-(2-(1H-1,2,4-triazol-1-yl)ethoxy)-4-chloro-5-((5-(furan-2-yl)thiazol-2-yl)methyl)phenyl)-6-(hydroxymethyl)-tetrahydro-2H-pyran-3,4,5-triol

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate / N,N-dimethyl-formamide / 60 h / 20 °C / Inert atmosphere

2: N,N-dimethyl-formamide / 15 h / 20 °C / Inert atmosphere

With caesium carbonate; In N,N-dimethyl-formamide;