HEXANE-2,5-DIONE MONOETHYLENEKETAL

Base Information

Chemical Name:HEXANE-2,5-DIONE MONOETHYLENEKETAL
CAS No.:33528-35-7
Molecular Formula:C8H14 O3
Molecular Weight:158.197
Hs Code.:2932999099
Mol file:33528-35-7.mol

Synonyms:2,5-Hexanedionemonoethylene ketal; 4-(2-Methyl[1,3]dioxolan-2-yl)butan-2-one

Suppliers and Price of HEXANE-2,5-DIONE MONOETHYLENEKETAL

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2,5-HexanedioneMonoethyleneKetal
1g
$ 145.00

TRC
2,5-HexanedioneMonoethyleneKetal
10g
$ 1165.00

Medical Isotopes, Inc.
Hexane-2,5-dioneMonoethyleneketal
1 g
$ 825.00

American Custom Chemicals Corporation
2,5-HEXANEDIONE MONOETHYLENE KETAL 95.00%
5MG
$ 502.71

Total 6 raw suppliers

Chemical Property of HEXANE-2,5-DIONE MONOETHYLENEKETAL

Chemical Property:

Boiling Point:48-53°C / 300-500 mtor
PSA：35.53000
Density:1.008±0.06 g/cm3(Predicted)
LogP:1.11860
Storage Temp.:Refrigerator
Solubility.:Acetonitrile (Sparingly), Chloroform (Slightly), Methanol

Purity/Quality:

98%Min ^*data from raw suppliers

2,5-HexanedioneMonoethyleneKetal ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses 2,5-Hexanedione Monoethylene Ketal is used in the synthesis of Dinordrin and analogs.

Technology Process of HEXANE-2,5-DIONE MONOETHYLENEKETAL

There total 1 articles about HEXANE-2,5-DIONE MONOETHYLENEKETAL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 497-26-7
2-methyl-1,3-dioxolane

: 78-94-4,25038-87-3
methyl vinyl ketone

: 33528-35-7
4-(2-methyl-1,3-dioxolan-2-yl)butan-2-one

: 542-59-6
2-hydroxyethyl acetate

Guidance literature:: With benzophenone; for 2.5h; Title compound not separated from byproducts; Irradiation;
DOI:10.1016/S0040-4020(01)01058-4

Reference yield: 70.0%

: 33528-35-7
4-(2-methyl-1,3-dioxolan-2-yl)butan-2-one

: 110-13-4
2,5-hexanedione

Guidance literature:: With sulfuric acid; In water; acetone; at 45 ℃; for 4h;
DOI:10.1016/S0040-4020(01)92014-9

Reference yield:

: 33528-35-7
4-(2-methyl-1,3-dioxolan-2-yl)butan-2-one

: 42137-04-2
5-hydroxy-5-methylhexan-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent Turnov_. / diethyl ether / 2 h / 20 °C

2: 94 percent Turnov_. / pyridinium p-toluene sulfonate (PPTS) / H₂O / acetone / 1) 48h, ca. 20 deg C, 2) 1h, 40 deg C

With pyridinium p-toluenesulfonate; water; In diethyl ether; acetone;
DOI:10.1007/BF00957783