methyl (2-bromo-3-phenylpropionyl-[2-tert-butyldimethylsilyloxy)benzyl]aminoacetate

Base Information

Chemical Name:methyl (2-bromo-3-phenylpropionyl-[2-tert-butyldimethylsilyloxy)benzyl]aminoacetate
CAS No.:716317-14-5
Molecular Formula:C₂₅H₃₄BrNO₄Si
Molecular Weight:520.539
Hs Code.:

Synonyms:methyl (2-bromo-3-phenylpropionyl-[2-tert-butyldimethylsilyloxy)benzyl]aminoacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (2-bromo-3-phenylpropionyl-[2-tert-butyldimethylsilyloxy)benzyl]aminoacetate

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Technology Process of methyl (2-bromo-3-phenylpropionyl-[2-tert-butyldimethylsilyloxy)benzyl]aminoacetate

There total 3 articles about methyl (2-bromo-3-phenylpropionyl-[2-tert-butyldimethylsilyloxy)benzyl]aminoacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 81136-07-4,42762-86-7
2-bromo-3-phenylpropionyl chloride

: 716317-13-4
methyl [2-(tert-butyldimethylsilyloxy)benzylamino]acetate

: 716317-14-5
methyl (2-bromo-3-phenylpropionyl-[2-tert-butyldimethylsilyloxy)benzyl]aminoacetate

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 16h;
DOI:10.3987/com-04-10022

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 716317-14-5
methyl (2-bromo-3-phenylpropionyl-[2-tert-butyldimethylsilyloxy)benzyl]aminoacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / diisopropylethylamine / CH₂Cl₂ / 22 h / 20 °C

2: 70 percent / triethylamine / CH₂Cl₂ / 16 h / 20 °C

With triethylamine; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.3987/com-04-10022

Reference yield:

: 182913-11-7
2-((3-methoxycarbonylmethylamino)methyl)phenol

: 716317-14-5
methyl (2-bromo-3-phenylpropionyl-[2-tert-butyldimethylsilyloxy)benzyl]aminoacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / diisopropylethylamine / CH₂Cl₂ / 22 h / 20 °C

2: 70 percent / triethylamine / CH₂Cl₂ / 16 h / 20 °C

With triethylamine; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.3987/com-04-10022