4-chloro-3-[(2,2-dimethyl-1,3-dioxolan-4-yl)methyl]-1-(4-methoxybenzyl)-1H-pyrazolo[3,4-d]pyrimidine-6-amine

Base Information

Chemical Name:4-chloro-3-[(2,2-dimethyl-1,3-dioxolan-4-yl)methyl]-1-(4-methoxybenzyl)-1H-pyrazolo[3,4-d]pyrimidine-6-amine
CAS No.:1015060-08-8
Molecular Formula:C₁₉H₂₂ClN₅O₃
Molecular Weight:403.868
Hs Code.:

Synonyms:4-chloro-3-[(2,2-dimethyl-1,3-dioxolan-4-yl)methyl]-1-(4-methoxybenzyl)-1H-pyrazolo[3,4-d]pyrimidine-6-amine

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Chemical Property of 4-chloro-3-[(2,2-dimethyl-1,3-dioxolan-4-yl)methyl]-1-(4-methoxybenzyl)-1H-pyrazolo[3,4-d]pyrimidine-6-amine

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Technology Process of 4-chloro-3-[(2,2-dimethyl-1,3-dioxolan-4-yl)methyl]-1-(4-methoxybenzyl)-1H-pyrazolo[3,4-d]pyrimidine-6-amine

There total 5 articles about 4-chloro-3-[(2,2-dimethyl-1,3-dioxolan-4-yl)methyl]-1-(4-methoxybenzyl)-1H-pyrazolo[3,4-d]pyrimidine-6-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1015057-85-8
1-(2-amino-4,6-dichloropyrimidin-5-yl)-2-(2,2-dimethyl-[1,3]dioxolan-4-yl)ethan-1-one

: 2011-48-5,412327-07-2
1-(4-methoxybenzyl)hydrazine hydrochloride

: 1015060-08-8
4-chloro-3-[(2,2-dimethyl-1,3-dioxolan-4-yl)methyl]-1-(4-methoxybenzyl)-1H-pyrazolo[3,4-d]pyrimidine-6-amine

Guidance literature:: With triethylamine; In dichloromethane; for 17.5h; Cooling with ice;

Reference yield:

: C₈H₁₁Cl₂N₃O₃

: 1015060-08-8
4-chloro-3-[(2,2-dimethyl-1,3-dioxolan-4-yl)methyl]-1-(4-methoxybenzyl)-1H-pyrazolo[3,4-d]pyrimidine-6-amine

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / N,N-dimethyl-formamide / 14 h / 20 °C

2: acetic anhydride; dimethyl sulfoxide / 18 h / 20 °C

3: triethylamine / dichloromethane / 17.5 h / Cooling with ice

With acetic anhydride; dimethyl sulfoxide; triethylamine; toluene-4-sulfonic acid; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 5604-46-6
2-amino-4,6-dichloropyrimidine-5-carboxaldehyde

: 1015060-08-8
4-chloro-3-[(2,2-dimethyl-1,3-dioxolan-4-yl)methyl]-1-(4-methoxybenzyl)-1H-pyrazolo[3,4-d]pyrimidine-6-amine

Guidance literature:: Multi-step reaction with 5 steps

1: sodium iodide; zinc; indium / N,N-dimethyl-formamide / 3 h

2: water; 4-methylmorpholine N-oxide / osmium(VIII) oxide / tetrahydrofuran; acetone / 48 h / 20 °C

3: toluene-4-sulfonic acid / N,N-dimethyl-formamide / 14 h / 20 °C

4: acetic anhydride; dimethyl sulfoxide / 18 h / 20 °C

5: triethylamine / dichloromethane / 17.5 h / Cooling with ice

With indium; water; acetic anhydride; dimethyl sulfoxide; 4-methylmorpholine N-oxide; triethylamine; sodium iodide; zinc; osmium(VIII) oxide; toluene-4-sulfonic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetone;