2-benzyl 1,4-di-tert-butyl-4-[2-(chloromethyl)-2-propenyl]-5-oxo-1,2,4-pyrrolidinetricarboxylate

Base Information

Chemical Name:2-benzyl 1,4-di-tert-butyl-4-[2-(chloromethyl)-2-propenyl]-5-oxo-1,2,4-pyrrolidinetricarboxylate
CAS No.:942603-38-5
Molecular Formula:C₂₆H₃₄ClNO₇
Molecular Weight:508.011
Hs Code.:

Synonyms:2-benzyl 1,4-di-tert-butyl-4-[2-(chloromethyl)-2-propenyl]-5-oxo-1,2,4-pyrrolidinetricarboxylate

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Chemical Property of 2-benzyl 1,4-di-tert-butyl-4-[2-(chloromethyl)-2-propenyl]-5-oxo-1,2,4-pyrrolidinetricarboxylate

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Technology Process of 2-benzyl 1,4-di-tert-butyl-4-[2-(chloromethyl)-2-propenyl]-5-oxo-1,2,4-pyrrolidinetricarboxylate

There total 3 articles about 2-benzyl 1,4-di-tert-butyl-4-[2-(chloromethyl)-2-propenyl]-5-oxo-1,2,4-pyrrolidinetricarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 861657-83-2
2-benzyl 1,4-di-t-butyl 5-oxo-1,2,4-pyrrolidinetricarboxylate

: 1871-57-4
2-chloromethyl-3-chloroprop-1-ene

: 942603-38-5
2-benzyl 1,4-di-tert-butyl-4-[2-(chloromethyl)-2-propenyl]-5-oxo-1,2,4-pyrrolidinetricarboxylate

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; Heating;
DOI:10.1016/j.tet.2007.03.084

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 942603-38-5
2-benzyl 1,4-di-tert-butyl-4-[2-(chloromethyl)-2-propenyl]-5-oxo-1,2,4-pyrrolidinetricarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: LiHMDS / tetrahydrofuran / 2 h / -78 °C

1.2: tetrahydrofuran / 20 °C

2.1: 60 percent / KOtBu / tetrahydrofuran / Heating

With potassium tert-butylate; lithium hexamethyldisilazane; In tetrahydrofuran;
DOI:10.1016/j.tet.2007.03.084

Reference yield:

: 113400-36-5,400626-71-3
(S)-2-benzyl 1-tert-butyl 5-oxopyrrolidine-1,2-dicarboxylate

: 942603-38-5
2-benzyl 1,4-di-tert-butyl-4-[2-(chloromethyl)-2-propenyl]-5-oxo-1,2,4-pyrrolidinetricarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: LiHMDS / tetrahydrofuran / 2 h / -78 °C

1.2: tetrahydrofuran / 20 °C

2.1: 60 percent / KOtBu / tetrahydrofuran / Heating

With potassium tert-butylate; lithium hexamethyldisilazane; In tetrahydrofuran;
DOI:10.1016/j.tet.2007.03.084