(+/-)-N-<2-<<<<2,6-bis(1-methylethyl)phenyl>amino>carbonyl>amino>-1-phenylethyl>-2-pyridinylamide

Base Information

Chemical Name:(+/-)-N-<2-<<<<2,6-bis(1-methylethyl)phenyl>amino>carbonyl>amino>-1-phenylethyl>-2-pyridinylamide
CAS No.:137102-24-0
Molecular Formula:C₁₄H₁₁N₃O
Molecular Weight:237.261
Hs Code.:

Synonyms:(+/-)-N-<2-<<<<2,6-bis(1-methylethyl)phenyl>amino>carbonyl>amino>-1-phenylethyl>-2-pyridinylamide

Suppliers and Price of (+/-)-N-<2-<<<<2,6-bis(1-methylethyl)phenyl>amino>carbonyl>amino>-1-phenylethyl>-2-pyridinylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-N-<2-<<<<2,6-bis(1-methylethyl)phenyl>amino>carbonyl>amino>-1-phenylethyl>-2-pyridinylamide

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Technology Process of (+/-)-N-<2-<<<<2,6-bis(1-methylethyl)phenyl>amino>carbonyl>amino>-1-phenylethyl>-2-pyridinylamide

There total 1 articles about (+/-)-N-<2-<<<<2,6-bis(1-methylethyl)phenyl>amino>carbonyl>amino>-1-phenylethyl>-2-pyridinylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 98-98-6
2-Picolinic acid

: 16750-42-8,41804-94-8
2-amino-2-phenylacetonitrile

: 137102-24-0
(+/-)-N-<2-<<<<2,6-bis(1-methylethyl)phenyl>amino>carbonyl>amino>-1-phenylethyl>-2-pyridinylamide

Guidance literature:: With 1,1'-carbonyldiimidazole; In tetrahydrofuran; for 24h; Ambient temperature;
DOI:10.1021/jm00038a010

Reference yield:

: 137102-24-0
(+/-)-N-<2-<<<<2,6-bis(1-methylethyl)phenyl>amino>carbonyl>amino>-1-phenylethyl>-2-pyridinylamide

: 137101-85-0
Pyridine-2-carboxylic acid (2-amino-1-phenyl-ethyl)-amide

Guidance literature:: With ammonia; hydrogen; ranney nickel; In methanol; under 2585.7 Torr; Ambient temperature;
DOI:10.1021/jm00038a010

Reference yield:

: 137102-24-0
(+/-)-N-<2-<<<<2,6-bis(1-methylethyl)phenyl>amino>carbonyl>amino>-1-phenylethyl>-2-pyridinylamide

: 1-Oxy-pyridine-2-carboxylic acid {2-[3-(2,6-diisopropyl-phenyl)-ureido]-1-phenyl-ethyl}-amide

Guidance literature:: Multi-step reaction with 3 steps

1: NH₃, H₂ / Ranney nickel / methanol / 2585.7 Torr / Ambient temperature

2: tetrahydrofuran / 2 h / Ambient temperature

3: 3-chloroperbenzoic acid (m-CPBA) / CH₂Cl₂ / Heating

With ammonia; hydrogen; 3-chloro-benzenecarboperoxoic acid; ranney nickel; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jm00038a010