4-Chloro-4'-methoxy-2-nitroazobenzene

Base Information

Chemical Name:4-Chloro-4'-methoxy-2-nitroazobenzene
CAS No.:84613-57-0
Molecular Formula:C13H10 Cl N3 O3
Molecular Weight:291.694
Hs Code.:
European Community (EC) Number:283-394-9
DSSTox Substance ID:DTXSID201214830
Nikkaji Number:J333.541K
Mol file:84613-57-0.mol

Synonyms:4-Chloro-4'-methoxy-2-nitroazobenzene;84613-57-0;EINECS 283-394-9;1-(4-Chloro-2-nitrophenyl)-2-(4-methoxyphenyl)diazene;YVBBYHMLWXNHCI-UHFFFAOYSA-N;DTXSID201214830;NS00059612

Suppliers and Price of 4-Chloro-4'-methoxy-2-nitroazobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of 4-Chloro-4'-methoxy-2-nitroazobenzene

Chemical Property:

Boiling Point:454.2oC at 760 mmHg
Flash Point:228.5oC
PSA：79.77000
Density:1.35g/cm3
LogP:5.19540
XLogP3:4.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:3
Exact Mass:291.0410689
Heavy Atom Count:20
Complexity:353

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=C(C=C1)N=NC2=C(C=C(C=C2)Cl)[N+](=O)[O-]

Technology Process of 4-Chloro-4'-methoxy-2-nitroazobenzene

There total 4 articles about 4-Chloro-4'-methoxy-2-nitroazobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 89284-65-1
4-chloro-2-nitro-1-nitrosobenzene

: 104-94-9
4-methoxy-aniline

: 84613-57-0
4-(2'-nitro-4'-chlorophenylazo)-anisole

Guidance literature:: In acetic acid; Ambient temperature;

Reference yield:

: 89-63-4
4-Chloro-2-nitroaniline

: 84613-57-0
4-(2'-nitro-4'-chlorophenylazo)-anisole

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaNO₂, H₂SO₄, 2.) 5percent aq. NaOH / 1.) acetic acid

2: MeONa / methanol / 3 h / Heating

With sodium hydroxide; sulfuric acid; sodium methylate; sodium nitrite; In methanol;

Reference yield:

: 108-95-2,27073-41-2
phenol

: 84613-57-0
4-(2'-nitro-4'-chlorophenylazo)-anisole

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaNO₂, H₂SO₄, 2.) 5percent aq. NaOH / 1.) acetic acid

2: MeONa / methanol / 3 h / Heating

With sodium hydroxide; sulfuric acid; sodium methylate; sodium nitrite; In methanol;