Technology Process of tert-butyl ((3R,6S)-6-(((1-phenyl-1H-tetrazol-5-yl)sulfonyl)-methyl)tetrahydro-2H-pyran-3-yl)carbamate
There total 7 articles about tert-butyl ((3R,6S)-6-(((1-phenyl-1H-tetrazol-5-yl)sulfonyl)-methyl)tetrahydro-2H-pyran-3-yl)carbamate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hexaammonium heptamolybdate tetrahydrate; dihydrogen peroxide;
In
tetrahydrofuran; ethanol; water;
at 20 - 65 ℃;
for 3h;
DOI:10.1021/jm400963y
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: hydrogen / platinum(IV) oxide / ethyl acetate / 3 h
2.1: dmap; triethylamine / dichloromethane / 4 h / 0 - 20 °C
3.1: sodium iodide / acetone / 24 h / Heating / reflux
4.1: potassium hydroxide / ethanol / 1 h / Heating / reflux
4.2: Heating / reflux
5.1: ammonium heptamolybdate; dihydrogen peroxide / tetrahydrofuran; ethanol; water / 3 h / 20 - 65 °C
With
dmap; ammonium heptamolybdate; potassium hydroxide; hydrogen; dihydrogen peroxide; triethylamine; sodium iodide;
platinum(IV) oxide;
In
tetrahydrofuran; ethanol; dichloromethane; water; ethyl acetate; acetone;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: water; acetic acid / tetrahydrofuran / 5 h / 70 °C
2.1: hydrogen / platinum(IV) oxide / ethyl acetate / 3 h
3.1: dmap; triethylamine / dichloromethane / 4 h / 0 - 20 °C
4.1: sodium iodide / acetone / 24 h / Heating / reflux
5.1: potassium hydroxide / ethanol / 1 h / Heating / reflux
5.2: Heating / reflux
6.1: ammonium heptamolybdate; dihydrogen peroxide / tetrahydrofuran; ethanol; water / 3 h / 20 - 65 °C
With
dmap; ammonium heptamolybdate; potassium hydroxide; water; hydrogen; dihydrogen peroxide; acetic acid; triethylamine; sodium iodide;
platinum(IV) oxide;
In
tetrahydrofuran; ethanol; dichloromethane; water; ethyl acetate; acetone;