4,4-difluoro-8-[3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenyl]-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene

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Chemical Name:4,4-difluoro-8-[3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenyl]-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene
CAS No.:1379793-95-9
Molecular Formula:C₄₀H₆₁BF₂N₂O₁₂
Molecular Weight:810.738
Hs Code.:

Synonyms:4,4-difluoro-8-[3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenyl]-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene

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Chemical Property of 4,4-difluoro-8-[3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenyl]-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene

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Technology Process of 4,4-difluoro-8-[3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenyl]-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene

There total 2 articles about 4,4-difluoro-8-[3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenyl]-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 866122-72-7
3,4,5-tris-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-benzaldehyde

: 625-82-1
2,4-dimethyl-1H-pyrrole

: 109-63-7
boron trifluoride diethyl etherate

: 118-75-2
chloranil

: 1379793-95-9
4,4-difluoro-8-[3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenyl]-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene

Guidance literature:: 3,4,5-tris-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-benzaldehyde; 2,4-dimethyl-1H-pyrrole; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 24h; Darkness;

chloranil; In dichloromethane; for 1h;

boron trifluoride diethyl etherate; Further stages;
DOI:10.1021/ol303306s

Reference yield: 56.0%

: 866122-72-7
3,4,5-tris-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-benzaldehyde

: 625-82-1
2,4-dimethyl-1H-pyrrole

: 1379793-95-9
4,4-difluoro-8-[3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenyl]-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene

Guidance literature:: 3,4,5-tris-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-benzaldehyde; 2,4-dimethyl-1H-pyrrole; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 18h; Inert atmosphere;

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; for 1.5h; Inert atmosphere;

With boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/ejoc.201101839