2-chloro-N-[2-(N,N-diethylamino)ethyl]-N-(2-nitrophenyl)-3-pyridinesulfonamide

Base Information

Chemical Name:2-chloro-N-[2-(N,N-diethylamino)ethyl]-N-(2-nitrophenyl)-3-pyridinesulfonamide
CAS No.:871715-15-0
Molecular Formula:C₁₇H₂₁ClN₄O₄S
Molecular Weight:412.897
Hs Code.:

Synonyms:2-chloro-N-[2-(N,N-diethylamino)ethyl]-N-(2-nitrophenyl)-3-pyridinesulfonamide

Suppliers and Price of 2-chloro-N-[2-(N,N-diethylamino)ethyl]-N-(2-nitrophenyl)-3-pyridinesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-chloro-N-[2-(N,N-diethylamino)ethyl]-N-(2-nitrophenyl)-3-pyridinesulfonamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-chloro-N-[2-(N,N-diethylamino)ethyl]-N-(2-nitrophenyl)-3-pyridinesulfonamide

There total 3 articles about 2-chloro-N-[2-(N,N-diethylamino)ethyl]-N-(2-nitrophenyl)-3-pyridinesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 733739-11-2
2-chloro-N-(2-nitrophenyl)-3-pyridinesulfonamide

: 869-24-9
2-chloro-N,N-diethylethylamine hydrochloride

: 871715-15-0
2-chloro-N-[2-(N,N-diethylamino)ethyl]-N-(2-nitrophenyl)-3-pyridinesulfonamide

Guidance literature:: With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; In toluene; for 20h; Heating;
DOI:10.1021/jm0503897

Reference yield:

: 6298-19-7
2-chloro-3-aminopyridine

: 871715-15-0
2-chloro-N-[2-(N,N-diethylamino)ethyl]-N-(2-nitrophenyl)-3-pyridinesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: aq. NaNO₂; HCl / 0.75 h / 0 °C

1.2: 72 percent / SO₂; CuCl₂; aq. AcOH / 1.5 h

2.1: 53 percent / pyridine / 2 h / 70 °C

3.1: 52 percent / aq. NaOH; benzyltriethylammonium chloride / toluene / 20 h / Heating

With pyridine; hydrogenchloride; sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; sodium nitrite; In toluene;
DOI:10.1021/jm0503897

Reference yield:

: 6684-06-6
2-chloro-3-pyridinesulfonyl chloride

: 871715-15-0
2-chloro-N-[2-(N,N-diethylamino)ethyl]-N-(2-nitrophenyl)-3-pyridinesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 53 percent / pyridine / 2 h / 70 °C

2: 52 percent / aq. NaOH; benzyltriethylammonium chloride / toluene / 20 h / Heating

With pyridine; sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; In toluene;
DOI:10.1021/jm0503897