C₇H₈O₃S*C₂₆H₂₈N₆O

Base Information

Chemical Name:C₇H₈O₃S*C₂₆H₂₈N₆O
CAS No.:1364799-92-7
Molecular Formula:C₇H₈O₃S*C₂₆H₂₈N₆O
Molecular Weight:612.753
Hs Code.:

C<sub>7</sub>H<sub>8</sub>O<sub>3</sub>S*C<sub>26</sub>H<sub>28</sub>N<sub>6</sub>O

Synonyms:C₇H₈O₃S*C₂₆H₂₈N₆O

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Chemical Property of C₇H₈O₃S*C₂₆H₂₈N₆O

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Technology Process of C₇H₈O₃S*C₂₆H₂₈N₆O

There total 12 articles about C₇H₈O₃S*C₂₆H₂₈N₆O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1254036-71-9
6-(1H-indol-4-yl)-4-(5-{[4-(1-methylethyl)-1-piperazinyl]methyl}-1,3-oxazol-2-yl)-1H-indazole

: 104-15-4
toluene-4-sulfonic acid

: 1364799-92-7
C₇H₈O₃S*C₂₆H₂₈N₆O

Guidance literature:: In acetonitrile;

Reference yield:

: 885519-56-2
6-chloro-4-iodo-1H-indazole

: 1364799-92-7
C₇H₈O₃S*C₂₆H₂₈N₆O

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.33 h / 10 °C / Cooling with ice; Inert atmosphere

1.2: 20 °C

2.1: triethylamine / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / xylene / 2 h / 150 °C

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide / N,N-dimethyl-formamide / 0.5 h / 100 °C / microwave irradiation

4.1: diisobutylaluminium hydride / dichloromethane / 3 h / -25 - -20 °C

5.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 3 h / 0 - 20 °C

6.1: dichloromethane / 1.25 h / 22 °C / Inert atmosphere

7.1: potassium phosphate / 2’-(dimethylamino)-2-biphenylyl-palladium(II)chloride dinorbornylphosphine complex / 1,4-dioxane; water / 1.5 h / 100 - 140 °C / microwave irradiation

8.1: acetonitrile

With potassium phosphate; carbon tetrabromide; sodium hydride; diisobutylaluminium hydride; triethylamine; triphenylphosphine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2’-(dimethylamino)-2-biphenylyl-palladium(II)chloride dinorbornylphosphine complex; In 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; xylene;

Reference yield:

: 1254036-94-6
6-chloro-4-iodo-1-(phenylsulfonyl)-1H-indazole

: 1364799-92-7
C₇H₈O₃S*C₂₆H₂₈N₆O

Guidance literature:: Multi-step reaction with 7 steps

1: triethylamine / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / xylene / 2 h / 150 °C

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide / N,N-dimethyl-formamide / 0.5 h / 100 °C / microwave irradiation

3: diisobutylaluminium hydride / dichloromethane / 3 h / -25 - -20 °C

4: carbon tetrabromide; triphenylphosphine / dichloromethane / 3 h / 0 - 20 °C

5: dichloromethane / 1.25 h / 22 °C / Inert atmosphere

6: potassium phosphate / 2’-(dimethylamino)-2-biphenylyl-palladium(II)chloride dinorbornylphosphine complex / 1,4-dioxane; water / 1.5 h / 100 - 140 °C / microwave irradiation

7: acetonitrile

With potassium phosphate; carbon tetrabromide; diisobutylaluminium hydride; triethylamine; triphenylphosphine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2’-(dimethylamino)-2-biphenylyl-palladium(II)chloride dinorbornylphosphine complex; In 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; xylene;