Technology Process of C51H58N4O2S3
There total 5 articles about C51H58N4O2S3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: toluene-4-sulfonic acid / benzene / Inert atmosphere; Schlenk technique
2: Trimethyl borate; hydrogenchloride; n-butyllithium / water / Inert atmosphere; Schlenk technique
3: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / tetrahydrofuran; water / 48 h / 80 °C / Inert atmosphere; Schlenk technique
4: N-Bromosuccinimide; acetic acid / chloroform / Inert atmosphere; Schlenk technique
5: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / tetrahydrofuran; water / Inert atmosphere; Schlenk technique
6: piperidine / chloroform / Inert atmosphere; Schlenk technique; Reflux
With
piperidine; hydrogenchloride; N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium(0); n-butyllithium; Trimethyl borate; sodium carbonate; toluene-4-sulfonic acid; acetic acid;
In
tetrahydrofuran; chloroform; water; benzene;
3: |Suzuki Coupling / 5: |Suzuki Coupling / 6: |Knoevenagel Condensation;
DOI:10.1016/j.dyepig.2012.10.002
- Guidance literature:
-
Multi-step reaction with 5 steps
1: Trimethyl borate; hydrogenchloride; n-butyllithium / water / Inert atmosphere; Schlenk technique
2: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / tetrahydrofuran; water / 48 h / 80 °C / Inert atmosphere; Schlenk technique
3: N-Bromosuccinimide; acetic acid / chloroform / Inert atmosphere; Schlenk technique
4: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / tetrahydrofuran; water / Inert atmosphere; Schlenk technique
5: piperidine / chloroform / Inert atmosphere; Schlenk technique; Reflux
With
piperidine; hydrogenchloride; N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium(0); n-butyllithium; Trimethyl borate; sodium carbonate; acetic acid;
In
tetrahydrofuran; chloroform; water;
2: |Suzuki Coupling / 4: |Suzuki Coupling / 5: |Knoevenagel Condensation;
DOI:10.1016/j.dyepig.2012.10.002