N-[4-chloro-2-tert-butyldimethylsilyloxy-3-(N,N-dimethylaminosulfonyl)phenyl]-N'-(2-bromophenyl)carbodiimide

Base Information

Chemical Name:N-[4-chloro-2-tert-butyldimethylsilyloxy-3-(N,N-dimethylaminosulfonyl)phenyl]-N'-(2-bromophenyl)carbodiimide
CAS No.:364363-04-2
Molecular Formula:C₂₁H₂₇BrClN₃O₃SSi
Molecular Weight:544.972
Hs Code.:

Synonyms:N-[4-chloro-2-tert-butyldimethylsilyloxy-3-(N,N-dimethylaminosulfonyl)phenyl]-N'-(2-bromophenyl)carbodiimide

Suppliers and Price of N-[4-chloro-2-tert-butyldimethylsilyloxy-3-(N,N-dimethylaminosulfonyl)phenyl]-N'-(2-bromophenyl)carbodiimide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-[4-chloro-2-tert-butyldimethylsilyloxy-3-(N,N-dimethylaminosulfonyl)phenyl]-N'-(2-bromophenyl)carbodiimide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-[4-chloro-2-tert-butyldimethylsilyloxy-3-(N,N-dimethylaminosulfonyl)phenyl]-N'-(2-bromophenyl)carbodiimide

There total 6 articles about N-[4-chloro-2-tert-butyldimethylsilyloxy-3-(N,N-dimethylaminosulfonyl)phenyl]-N'-(2-bromophenyl)carbodiimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 364363-02-0
N-[4-chloro-2-tert-butyldimethylsilyloxy-3-(N,N-dimethylaminosulfonyl)phenyl]-N'-(2-bromophenyl) thiourea

: 1122-58-3
dmap

: 124-63-0
methanesulfonyl chloride

: 364363-04-2
N-[4-chloro-2-tert-butyldimethylsilyloxy-3-(N,N-dimethylaminosulfonyl)phenyl]-N'-(2-bromophenyl)carbodiimide

Guidance literature:: With triethylamine; In dichloromethane;

Reference yield:

: 364363-02-0
N-[4-chloro-2-tert-butyldimethylsilyloxy-3-(N,N-dimethylaminosulfonyl)phenyl]-N'-(2-bromophenyl) thiourea

: 364363-04-2
N-[4-chloro-2-tert-butyldimethylsilyloxy-3-(N,N-dimethylaminosulfonyl)phenyl]-N'-(2-bromophenyl)carbodiimide

Guidance literature:: With methanesulfonyl chloride; triethylamine; at 20 ℃;
DOI:10.1016/j.bmcl.2006.08.042

Reference yield:

: 361393-21-7
N-[4-chloro-2-hydroxy-3-(N'',N''-dimethylaminosulfonyl)phenyl]-N'-(2-bromophenyl)-thiourea

: 364363-04-2
N-[4-chloro-2-tert-butyldimethylsilyloxy-3-(N,N-dimethylaminosulfonyl)phenyl]-N'-(2-bromophenyl)carbodiimide

Guidance literature:: Multi-step reaction with 2 steps

1: imidazole / CH₂Cl₂ / 20 °C

2: MsCl; Et₃N / 20 °C

With 1H-imidazole; methanesulfonyl chloride; triethylamine; In dichloromethane;
DOI:10.1016/j.bmcl.2006.08.042