methyl 4-(N,N-bis(2-(trimethylsilyl)-ethoxymethyl)sulfamoyl)-3-(4((2',6'-dimethyl-4'-(3-(methylsulfonyl)propoxy)-[1,1'-biphenyl]-3-yl)methoxy)phenyl)butanoate

Base Information

Chemical Name:methyl 4-(N,N-bis(2-(trimethylsilyl)-ethoxymethyl)sulfamoyl)-3-(4((2',6'-dimethyl-4'-(3-(methylsulfonyl)propoxy)-[1,1'-biphenyl]-3-yl)methoxy)phenyl)butanoate
CAS No.:1372195-74-8
Molecular Formula:C₄₂H₆₅NO₁₀S₂Si₂
Molecular Weight:864.282
Hs Code.:

methyl 4-(N,N-bis(2-(trimethylsilyl)-ethoxymethyl)sulfamoyl)-3-(4((2',6'-dimethyl-4'-(3-(methylsulfonyl)propoxy)-[1,1'-biphenyl]-3-yl)methoxy)phenyl)butanoate

Synonyms:methyl 4-(N,N-bis(2-(trimethylsilyl)-ethoxymethyl)sulfamoyl)-3-(4((2',6'-dimethyl-4'-(3-(methylsulfonyl)propoxy)-[1,1'-biphenyl]-3-yl)methoxy)phenyl)butanoate

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Chemical Property of methyl 4-(N,N-bis(2-(trimethylsilyl)-ethoxymethyl)sulfamoyl)-3-(4((2',6'-dimethyl-4'-(3-(methylsulfonyl)propoxy)-[1,1'-biphenyl]-3-yl)methoxy)phenyl)butanoate

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Technology Process of methyl 4-(N,N-bis(2-(trimethylsilyl)-ethoxymethyl)sulfamoyl)-3-(4((2',6'-dimethyl-4'-(3-(methylsulfonyl)propoxy)-[1,1'-biphenyl]-3-yl)methoxy)phenyl)butanoate

There total 7 articles about methyl 4-(N,N-bis(2-(trimethylsilyl)-ethoxymethyl)sulfamoyl)-3-(4((2',6'-dimethyl-4'-(3-(methylsulfonyl)propoxy)-[1,1'-biphenyl]-3-yl)methoxy)phenyl)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1372195-73-7
dimethyl 2-(2-(N,N-bis(2-(trimethylsilyl)ethoxymethyl)sulfamoyl)-1-(4-((2',6'-dimethyl-4'-(3-(methylsulfonyl)propoxy)-[1,1'-biphenyl]-3-yl)methoxy)phenyl)ethyl)malonate

: 1372195-74-8
methyl 4-(N,N-bis(2-(trimethylsilyl)-ethoxymethyl)sulfamoyl)-3-(4((2',6'-dimethyl-4'-(3-(methylsulfonyl)propoxy)-[1,1'-biphenyl]-3-yl)methoxy)phenyl)butanoate

Guidance literature:: With sodium chloride; In N,N-dimethyl-formamide; for 17h; Reflux;

Reference yield:

: 1000413-85-3
(2’,6’-dimethyl-4’-(3-(methylsulfonyl)propoxy)-[1,1‘-biphenyl]-3-yl)methanol

: 1372195-74-8
methyl 4-(N,N-bis(2-(trimethylsilyl)-ethoxymethyl)sulfamoyl)-3-(4((2',6'-dimethyl-4'-(3-(methylsulfonyl)propoxy)-[1,1'-biphenyl]-3-yl)methoxy)phenyl)butanoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: sulfuric acid; hydrogen bromide / 3.5 h / 60 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C / Inert atmosphere

3.1: lithium hexamethyldisilazane / tetrahydrofuran / Cooling

3.2: Cooling

3.3: 20 °C / Cooling

4.1: sodium methylate / tetrahydrofuran; methanol / 0.17 h / 20 °C

4.2: 65 h / Reflux

5.1: sodium chloride / N,N-dimethyl-formamide / 17 h / Reflux

With sulfuric acid; hydrogen bromide; sodium methylate; potassium carbonate; sodium chloride; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;

Reference yield:

: 76513-69-4
(2-trimethylethylsilylethoxy)methyl chloride

: 1372195-74-8
methyl 4-(N,N-bis(2-(trimethylsilyl)-ethoxymethyl)sulfamoyl)-3-(4((2',6'-dimethyl-4'-(3-(methylsulfonyl)propoxy)-[1,1'-biphenyl]-3-yl)methoxy)phenyl)butanoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / N,N-dimethyl-formamide

1.2: 2 h / 20 °C

2.1: lithium hexamethyldisilazane / tetrahydrofuran / Cooling

2.2: Cooling

2.3: 20 °C / Cooling

3.1: sodium methylate / tetrahydrofuran; methanol / 0.17 h / 20 °C

3.2: 65 h / Reflux

4.1: sodium chloride / N,N-dimethyl-formamide / 17 h / Reflux

With sodium methylate; sodium hydride; sodium chloride; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;