Technology Process of C32H34N6O3
There total 7 articles about C32H34N6O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
N-(3,5-dimethoxyphenyl)-3-(1-methyl-1H-pyrazol-4-yl)quinoxaline-6-amine;
With
sodium hydride;
In
N,N-dimethyl-formamide; mineral oil;
at 5 ℃;
for 0.5h;
4-(phenylmethyl)-2-morpholinemethanol methanesulfonate;
In
N,N-dimethyl-formamide; mineral oil;
at 60 ℃;
for 18h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: trichlorophosphate / 2 h / 100 °C
1.2: Cooling with ice
2.1: sodium carbonate / triphenylphosphine; palladium diacetate / 1,2-dimethoxyethane; water / 4 h / Reflux
3.1: sodium t-butanolate / palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / 1,4-dioxane / 90 °C / Inert atmosphere
4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 5 °C
4.2: 18 h / 60 °C
With
sodium hydride; sodium carbonate; sodium t-butanolate; trichlorophosphate;
palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triphenylphosphine;
In
1,4-dioxane; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide; mineral oil;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium carbonate / triphenylphosphine; palladium diacetate / 1,2-dimethoxyethane; water / 4 h / Reflux
2.1: sodium t-butanolate / palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / 1,4-dioxane / 90 °C / Inert atmosphere
3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 5 °C
3.2: 18 h / 60 °C
With
sodium hydride; sodium carbonate; sodium t-butanolate;
palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triphenylphosphine;
In
1,4-dioxane; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide; mineral oil;