(C₆H₅)2P(BH₃)CH₂CO₂CH₃

Base Information

Chemical Name:(C₆H₅)2P(BH₃)CH₂CO₂CH₃
CAS No.:127686-71-9
Molecular Formula:C₁₅H₁₈BO₂P
Molecular Weight:272.091
Hs Code.:

(C<sub>6</sub>H<sub>5</sub>)2P(BH<sub>3</sub>)CH<sub>2</sub>CO<sub>2</sub>CH<sub>3</sub>

Synonyms:(C₆H₅)2P(BH₃)CH₂CO₂CH₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (C₆H₅)2P(BH₃)CH₂CO₂CH₃

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Technology Process of (C₆H₅)2P(BH₃)CH₂CO₂CH₃

There total 2 articles about (C₆H₅)2P(BH₃)CH₂CO₂CH₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 616-38-6
carbonic acid dimethyl ester

: 54067-17-3
diphenylmethylphosphine-borane complex

: 127686-71-9
(C₆H₅)2P(BH₃)CH₂CO₂CH₃

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; pentane; argon atmosphere; addn. of lithium diisopropylamide in pentane to soln. of Ph2MePBH3 in THF (-78°C), standig (-78°C, 2 h), addn. of (MeO)2CO, stirring (0.5 h); treatment with aq. HCl, extn. (ether), drying of extracts (MgSO4), preparative TLC (silica gel);
DOI:10.1021/ja00169a036

Reference yield: 79.0%

: 96-34-4
methyl chloroacetate

: 41593-58-2
diphenylphosphineborane

: 127686-71-9
(C₆H₅)2P(BH₃)CH₂CO₂CH₃

Guidance literature:: With potassium hydroxide; In methanol; 0°C, stirring; treatment with aq. HCl, extn. (ether), preparative TLC;
DOI:10.1021/ja00169a036