carbamic acid 2-fluoro-1-phenyl-3-(4-phenyl-piperazin-1-yl)-propyl ester

Base Information

Chemical Name:carbamic acid 2-fluoro-1-phenyl-3-(4-phenyl-piperazin-1-yl)-propyl ester
CAS No.:1083076-58-7
Molecular Formula:C₂₀H₂₄FN₃O₂
Molecular Weight:357.428
Hs Code.:

Synonyms:carbamic acid 2-fluoro-1-phenyl-3-(4-phenyl-piperazin-1-yl)-propyl ester

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Chemical Property of carbamic acid 2-fluoro-1-phenyl-3-(4-phenyl-piperazin-1-yl)-propyl ester

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Technology Process of carbamic acid 2-fluoro-1-phenyl-3-(4-phenyl-piperazin-1-yl)-propyl ester

There total 6 articles about carbamic acid 2-fluoro-1-phenyl-3-(4-phenyl-piperazin-1-yl)-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₉H₂₃FN₂O

: 530-62-1
1,1'-carbonyldiimidazole

: 1083076-58-7
carbamic acid 2-fluoro-1-phenyl-3-(4-phenyl-piperazin-1-yl)-propyl ester

Guidance literature:: C₁₉H₂₃FN₂O; 1,1'-carbonyldiimidazole; In tetrahydrofuran; at 20 ℃; for 2h;

With ammonia; In tetrahydrofuran; water; at 20 ℃; for 2h;

Reference yield:

: 92-54-6
4-phenyl-1-piperazine

: 1083076-58-7
carbamic acid 2-fluoro-1-phenyl-3-(4-phenyl-piperazin-1-yl)-propyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogenchloride / water / 24 h / pH 2 - 3 / Heating / reflux

2.1: cyclohexanelithium diimide / tetrahydrofuran / 0.67 h / -78 - 0 °C

2.2: 2 h / -78 - 20 °C

3.1: sodium tetrahydroborate / methanol / 1 h / 20 °C

4.1: tetrahydrofuran / 2 h / 20 °C

4.2: 2 h / 20 °C

With hydrogenchloride; sodium tetrahydroborate; In tetrahydrofuran; methanol; water;

Reference yield:

: 26108-53-2
1-phenyl-3-(4-phenyl-1-piperazinyl)-1-propanone

: 1083076-58-7
carbamic acid 2-fluoro-1-phenyl-3-(4-phenyl-piperazin-1-yl)-propyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: cyclohexanelithium diimide / tetrahydrofuran / 0.67 h / -78 - 0 °C

1.2: 2 h / -78 - 20 °C

2.1: sodium tetrahydroborate / methanol / 1 h / 20 °C

3.1: tetrahydrofuran / 2 h / 20 °C

3.2: 2 h / 20 °C

With sodium tetrahydroborate; In tetrahydrofuran; methanol;