N-(4-Methoxy-benzyl)-N-[(4-methoxy-benzylcarbamoyl)-methyl]-2-(triphenyl-λ⁵-phosphanylidene)-acetamide

Base Information

• Chemical Name: N-(4-Methoxy-benzyl)-N-[(4-methoxy-benzylcarbamoyl)-methyl]-2-(triphenyl-λ⁵-phosphanylidene)-acetamide
• CAS No.: 144581-88-4
• Molecular Formula: C₃₈H₃₇N₂O₄P
• Molecular Weight: 616.697

Synonyms:N-(4-Methoxy-benzyl)-N-[(4-methoxy-benzylcarbamoyl)-methyl]-2-(triphenyl-λ⁵-phosphanylidene)-acetamide

Chemical Property of N-(4-Methoxy-benzyl)-N-[(4-methoxy-benzylcarbamoyl)-methyl]-2-(triphenyl-λ⁵-phosphanylidene)-acetamide

Chemical Property:

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Technology Process of N-(4-Methoxy-benzyl)-N-[(4-methoxy-benzylcarbamoyl)-methyl]-2-(triphenyl-λ⁵-phosphanylidene)-acetamide

There total 5 articles about N-(4-Methoxy-benzyl)-N-[(4-methoxy-benzylcarbamoyl)-methyl]-2-(triphenyl-λ⁵-phosphanylidene)-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

({(4-Methoxy-benzyl)-[(4-methoxy-benzylcarbamoyl)-methyl]-carbamoyl}-methyl)-triphenyl-phosphonium; bromide (144775-07-5) → N-(4-Methoxy-benzyl)-N-[(4-methoxy-benzylcarbamoyl)-methyl]-2-(triphenyl-λ5-phosphanylidene)-acetamide (144581-88-4)

Guidance literature:

With sodium hydroxide; In water;

DOI:10.1016/S0040-4039(00)79110-6

Reference yield:

N,N'-bis(p-methoxybenzyl)-α-aminoacetamide (117471-50-8) → N-(4-Methoxy-benzyl)-N-[(4-methoxy-benzylcarbamoyl)-methyl]-2-(triphenyl-λ5-phosphanylidene)-acetamide (144581-88-4)

Guidance literature:

Multi-step reaction with 3 steps

1: 99 percent / DCC

2: 98 percent

3: 100 percent / NaOH / H₂O

With sodium hydroxide; dicyclohexyl-carbodiimide; In water;

DOI:10.1016/S0040-4039(00)79110-6

Reference yield:

4-methoxy-benzylamine (2393-23-9) → N-(4-Methoxy-benzyl)-N-[(4-methoxy-benzylcarbamoyl)-methyl]-2-(triphenyl-λ5-phosphanylidene)-acetamide (144581-88-4)

Guidance literature:

Multi-step reaction with 4 steps

1: 96 percent

2: 99 percent / DCC

3: 98 percent

4: 100 percent / NaOH / H₂O

With sodium hydroxide; dicyclohexyl-carbodiimide; In water;

DOI:10.1016/S0040-4039(00)79110-6

upstream raw materials:

({(4-Methoxy-benzyl)-[(4-methoxy-benzylcarbamoyl)-methyl]-carbamoyl}-methyl)-triphenyl-phosphonium; bromide

N,N'-bis(p-methoxybenzyl)-α-aminoacetamide

4-methoxy-benzylamine

α-Bromo-N-p-methoxybenzylacetamide

Downstream raw materials:

5-Benzyloxy-3-oxo-2-(triphenyl-λ⁵-phosphanylidene)-pentanoic acid (4-methoxy-benzyl)-[(4-methoxy-benzylcarbamoyl)-methyl]-amide

3-(3-Benzyloxy-propionyl)-3-(tert-butyl-dimethyl-silanyloxy)-1,4-bis-(4-methoxy-benzyl)-piperazine-2,5-dione

(R)-3-((S)-3-Benzyloxy-1-hydroxy-propyl)-3-(tert-butyl-dimethyl-silanyloxy)-1,4-bis-(4-methoxy-benzyl)-piperazine-2,5-dione

3-(3-Benzyloxy-propionyl)-3-hydroxy-1,4-bis-(4-methoxy-benzyl)-piperazine-2,5-dione

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