Technology Process of C17H11N3O2
There total 6 articles about C17H11N3O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C18H13N3O2;
With
water; sodium carbonate;
In
1,4-dioxane;
at 80 ℃;
With
hydrogenchloride; water;
In
1,4-dioxane;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: acetic acid / water / 21 h / 100 °C
2.1: sulfuric acid / 30 h / Heating / reflux
3.1: trichlorophosphate / 0.5 h / 0 °C
3.2: 12 h / 20 °C
4.1: formic acid; hydroxylamine hydrochloride; sodium formate / 0.75 h / Heating / reflux
5.1: water; sodium carbonate / 1,4-dioxane / 80 °C
With
formic acid; hydroxylamine hydrochloride; water; sodium formate; sodium carbonate; acetic acid; trichlorophosphate;
sulfuric acid;
In
1,4-dioxane; water;
3.2: Vilsmeier Formylation;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: acetic acid / water / 21 h / 100 °C
2.1: sulfuric acid / 30 h / Heating / reflux
3.1: trichlorophosphate / 0.5 h / 0 °C
3.2: 12 h / 20 °C
4.1: formic acid; hydroxylamine hydrochloride; sodium formate / 0.75 h / Heating / reflux
5.1: water; sodium carbonate / 1,4-dioxane / 80 °C
With
formic acid; hydroxylamine hydrochloride; water; sodium formate; sodium carbonate; acetic acid; trichlorophosphate;
sulfuric acid;
In
1,4-dioxane; water;
3.2: Vilsmeier Formylation;