phenyl(5,10,15,20-tetrakis(p-tolyl)porphyrinato)iridium(III)

Base Information

Chemical Name:phenyl(5,10,15,20-tetrakis(p-tolyl)porphyrinato)iridium(III)
CAS No.:1224699-27-7
Molecular Formula:C₅₄H₄₁IrN₄
Molecular Weight:938.166
Hs Code.:

Synonyms:phenyl(5,10,15,20-tetrakis(p-tolyl)porphyrinato)iridium(III)

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Chemical Property of phenyl(5,10,15,20-tetrakis(p-tolyl)porphyrinato)iridium(III)

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Technology Process of phenyl(5,10,15,20-tetrakis(p-tolyl)porphyrinato)iridium(III)

There total 36 articles about phenyl(5,10,15,20-tetrakis(p-tolyl)porphyrinato)iridium(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 108-86-1,52753-63-6
bromobenzene

: 872415-81-1
(5,10,15,20-tetrakis(p-tolyl)porphyrinato)carbonyliridium(III) chloride

: 1224699-27-7
phenyl(5,10,15,20-tetrakis(p-tolyl)porphyrinato)iridium(III)

Guidance literature:: With K₂CO₃; In benzene; mixing Ir complex, PhBr, K2CO3 (20 equiv.), C6H6, 200°C, 2 d;
DOI:10.1021/om200027q

Reference yield: 99.0%

: 591-50-4
iodobenzene

: 872415-81-1
(5,10,15,20-tetrakis(p-tolyl)porphyrinato)carbonyliridium(III) chloride

: 1224699-27-7
phenyl(5,10,15,20-tetrakis(p-tolyl)porphyrinato)iridium(III)

Guidance literature:: With sodium hydroxide; In benzene; at 150 ℃; for 12h; Inert atmosphere; Darkness;
DOI:10.1021/om200251k

Reference yield: 75.0%

: 872415-81-1
(5,10,15,20-tetrakis(p-tolyl)porphyrinato)carbonyliridium(III) chloride

: 108-90-7
chlorobenzene

: 1224699-27-7
phenyl(5,10,15,20-tetrakis(p-tolyl)porphyrinato)iridium(III)

: 1,4-bis[ (5,10,15,20-tetrakis(p-tolyl)porphyrinato)iridium(III)] benzene

Guidance literature:: With K₂CO₃; In benzene; byproducts: 1,4-dichlorobenzene; heating of Ir(C20H8N4(p-tol)4)(CO)Cl, K2CO3, PhCl (200 equiv.) and benzene in Teflon screw capped Schlenk tube at 200°C under N2 for 7 h; monitoring by NMR and GC-MS;
DOI:10.1021/om200618m