4-azido-benzoic acid 2-benzyloxyacetyl-3,5-bis-(tert-butyl-diphenyl-silanyloxy)-phenyl ester

Base Information

Chemical Name:4-azido-benzoic acid 2-benzyloxyacetyl-3,5-bis-(tert-butyl-diphenyl-silanyloxy)-phenyl ester
CAS No.:322405-76-5
Molecular Formula:C₅₄H₅₃N₃O₆Si₂
Molecular Weight:896.202
Hs Code.:

4-azido-benzoic acid 2-benzyloxyacetyl-3,5-bis-(<i>tert</i>-butyl-diphenyl-silanyloxy)-phenyl ester

Synonyms:4-azido-benzoic acid 2-benzyloxyacetyl-3,5-bis-(tert-butyl-diphenyl-silanyloxy)-phenyl ester

Suppliers and Price of 4-azido-benzoic acid 2-benzyloxyacetyl-3,5-bis-(tert-butyl-diphenyl-silanyloxy)-phenyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-azido-benzoic acid 2-benzyloxyacetyl-3,5-bis-(tert-butyl-diphenyl-silanyloxy)-phenyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-azido-benzoic acid 2-benzyloxyacetyl-3,5-bis-(tert-butyl-diphenyl-silanyloxy)-phenyl ester

There total 4 articles about 4-azido-benzoic acid 2-benzyloxyacetyl-3,5-bis-(tert-butyl-diphenyl-silanyloxy)-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 6427-66-3
4-azidobenzoic acid

: 322405-73-2
2-benzyloxy-1-[2,4-bis-(tert-butyl-diphenyl-silanyloxy)-6-hydroxy-phenyl]-ethanone

: 322405-76-5
4-azido-benzoic acid 2-benzyloxyacetyl-3,5-bis-(tert-butyl-diphenyl-silanyloxy)-phenyl ester

Guidance literature:: With dmap; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;
DOI:10.1016/S0040-4039(00)01767-6

Reference yield:

: 108-73-6
3,5-dihydroxyphenol

: 322405-76-5
4-azido-benzoic acid 2-benzyloxyacetyl-3,5-bis-(tert-butyl-diphenyl-silanyloxy)-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / HCl / diethyl ether

2: 85 percent / Et₃N / CH₂Cl₂ / 20 °C

3: 71 percent / 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride; DMAP; p-TsOH / CH₂Cl₂

With hydrogenchloride; dmap; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In diethyl ether; dichloromethane;
DOI:10.1016/S0040-4039(00)01767-6

Reference yield:

: 13620-31-0
benzyloxyacetonitrile

: 322405-76-5
4-azido-benzoic acid 2-benzyloxyacetyl-3,5-bis-(tert-butyl-diphenyl-silanyloxy)-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / HCl / diethyl ether

2: 85 percent / Et₃N / CH₂Cl₂ / 20 °C

3: 71 percent / 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride; DMAP; p-TsOH / CH₂Cl₂

With hydrogenchloride; dmap; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In diethyl ether; dichloromethane;
DOI:10.1016/S0040-4039(00)01767-6