4,4-[1,3-propanediylbis(oxy)]bisbenzyl chloride

Base Information

Chemical Name:4,4-[1,3-propanediylbis(oxy)]bisbenzyl chloride
CAS No.:93408-26-5
Molecular Formula:C₁₇H₁₈Cl₂O₂
Molecular Weight:325.235
Hs Code.:

Synonyms:4,4-[1,3-propanediylbis(oxy)]bisbenzyl chloride

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Chemical Property of 4,4-[1,3-propanediylbis(oxy)]bisbenzyl chloride

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Technology Process of 4,4-[1,3-propanediylbis(oxy)]bisbenzyl chloride

There total 4 articles about 4,4-[1,3-propanediylbis(oxy)]bisbenzyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 32449-07-3
4,4'-<1,3-Propanediylbis(oxy)>bis(benzenemethanol)

: 93408-26-5
4,4-[1,3-propanediylbis(oxy)]bisbenzyl chloride

Guidance literature:: With thionyl chloride; In dichloromethane; at 0 ℃; for 5h; Inert atmosphere; Reflux;
DOI:10.1021/acsmedchemlett.8b00389

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 93408-26-5
4,4-[1,3-propanediylbis(oxy)]bisbenzyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 0 - 90 °C

1.2: 1 h / 90 °C

2.1: sodium tetrahydroborate / methanol; tetrahydrofuran / 6 h / 0 - 20 °C

3.1: thionyl chloride / dichloromethane / 5 h / 0 °C / Inert atmosphere; Reflux

With sodium tetrahydroborate; thionyl chloride; potassium carbonate; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/acsmedchemlett.8b00389

Reference yield:

: 3722-80-3
1,3-bis(4-formylphenoxy)propane

: 93408-26-5
4,4-[1,3-propanediylbis(oxy)]bisbenzyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol; tetrahydrofuran / 6 h / 0 - 20 °C

2: thionyl chloride / dichloromethane / 5 h / 0 °C / Inert atmosphere; Reflux

With sodium tetrahydroborate; thionyl chloride; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/acsmedchemlett.8b00389