1-fluoro-4-(1-methoxy-D-glucopyranos-1-yl)-2-(4-triisopropylsilylethynyl-benzyl)-benzene

Base Information

Chemical Name:1-fluoro-4-(1-methoxy-D-glucopyranos-1-yl)-2-(4-triisopropylsilylethynyl-benzyl)-benzene
CAS No.:864070-28-0
Molecular Formula:C₃₁H₄₃FO₆Si
Molecular Weight:558.763
Hs Code.:

Synonyms:1-fluoro-4-(1-methoxy-D-glucopyranos-1-yl)-2-(4-triisopropylsilylethynyl-benzyl)-benzene

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Chemical Property of 1-fluoro-4-(1-methoxy-D-glucopyranos-1-yl)-2-(4-triisopropylsilylethynyl-benzyl)-benzene

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Technology Process of 1-fluoro-4-(1-methoxy-D-glucopyranos-1-yl)-2-(4-triisopropylsilylethynyl-benzyl)-benzene

There total 4 articles about 1-fluoro-4-(1-methoxy-D-glucopyranos-1-yl)-2-(4-triisopropylsilylethynyl-benzyl)-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: C₄₃H₇₅FO₆Si₅

: 864070-28-0
1-fluoro-4-(1-methoxy-D-glucopyranos-1-yl)-2-(4-triisopropylsilylethynyl-benzyl)-benzene

Guidance literature:: C₄₃H₇₅FO₆Si₅; With methanesulfonic acid; In methanol; at 20 ℃; for 16h;

With N-ethyl-N,N-diisopropylamine; In methanol;

Reference yield: 50.0%

: 67-56-1
methanol

: 864070-28-0
1-fluoro-4-(1-methoxy-D-glucopyranos-1-yl)-2-(4-triisopropylsilylethynyl-benzyl)-benzene

Guidance literature:: [4-(5-bromo-2-fluoro-benzyl)-phenylethynyl]-triisopropyl-silane; With tert.-butyl lithium; In diethyl ether; pentane; at -80 ℃; for 0.75h;

(3R,4S,5R,6R)-3,4,5-tris((trimethylsilyl)oxy)-6-(((trimethylsilyl)oxy)methyl)tetrahydro-2H-pyran-2-one; In diethyl ether; pentane; at -80 - -78 ℃; for 3h;

methanol; With methanesulfonic acid; In diethyl ether; pentane; at -78 - 20 ℃; for 16h;

Reference yield: 50.0%

: 864070-24-6
[4-(5-bromo-2-fluoro-benzyl)-phenylethynyl]-triisopropyl-silane

: 75-75-2,98527-29-8
methanesulfonic acid

: 32469-28-6,55515-28-1,55515-29-2,32384-65-9
(3R,4S,5R,6R)-3,4,5-tris((trimethylsilyl)oxy)-6-(((trimethylsilyl)oxy)methyl)tetrahydro-2H-pyran-2-one

: 864070-28-0
1-fluoro-4-(1-methoxy-D-glucopyranos-1-yl)-2-(4-triisopropylsilylethynyl-benzyl)-benzene

Guidance literature:: [4-(5-bromo-2-fluoro-benzyl)-phenylethynyl]-triisopropyl-silane; With tert.-butyl lithium; In diethyl ether; pentane; at -80 ℃; for 0.75h;

(3R,4S,5R,6R)-3,4,5-tris((trimethylsilyl)oxy)-6-(((trimethylsilyl)oxy)methyl)tetrahydro-2H-pyran-2-one; In diethyl ether; pentane; at -80 - -78 ℃; for 3h;

methanesulfonic acid; With methanol; N-ethyl-N,N-diisopropylamine; more than 3 stages;