3,3'-bis(chloromethyl)-5,5'-di-tert-butyl-2,2'-dimethoxy-1,3-diphenylpropane

Base Information

Chemical Name:3,3'-bis(chloromethyl)-5,5'-di-tert-butyl-2,2'-dimethoxy-1,3-diphenylpropane
CAS No.:125665-98-7
Molecular Formula:C₂₇H₃₈Cl₂O₂
Molecular Weight:465.504
Hs Code.:

Synonyms:3,3'-bis(chloromethyl)-5,5'-di-tert-butyl-2,2'-dimethoxy-1,3-diphenylpropane

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Chemical Property of 3,3'-bis(chloromethyl)-5,5'-di-tert-butyl-2,2'-dimethoxy-1,3-diphenylpropane

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Technology Process of 3,3'-bis(chloromethyl)-5,5'-di-tert-butyl-2,2'-dimethoxy-1,3-diphenylpropane

There total 3 articles about 3,3'-bis(chloromethyl)-5,5'-di-tert-butyl-2,2'-dimethoxy-1,3-diphenylpropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 108656-63-9
1,3-bis(5-tert-butyl-2-methoxyphenyl)propane

: 125665-98-7
3,3'-bis(chloromethyl)-5,5'-di-tert-butyl-2,2'-dimethoxy-1,3-diphenylpropane

Guidance literature:: With hydrogenchloride; phosphoric acid; In acetic acid; at 90 - 95 ℃; for 36h;

Reference yield:

: 5396-38-3
1-(tert-butyl)-4-methoxybenzene

: 125665-98-7
3,3'-bis(chloromethyl)-5,5'-di-tert-butyl-2,2'-dimethoxy-1,3-diphenylpropane

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / Br₂ / CCl₄

2: 1) Mg, I₂, 2) CuBr, HMPA / 1) THF, reflux, 12 h, 2) reflux, 17 h

3: 99 percent / 36percent conc. HCl, H₃PO₄ / acetic acid / 36 h / 90 - 95 °C

With hydrogenchloride; N,N,N,N,N,N-hexamethylphosphoric triamide; phosphoric acid; bromine; iodine; magnesium; copper(I) bromide; In tetrachloromethane; acetic acid;

Reference yield:

: 41280-65-3
2-bromo-4-tert-butylanisole

: 125665-98-7
3,3'-bis(chloromethyl)-5,5'-di-tert-butyl-2,2'-dimethoxy-1,3-diphenylpropane

Guidance literature:: Multi-step reaction with 2 steps

1: 1) Mg, I₂, 2) CuBr, HMPA / 1) THF, reflux, 12 h, 2) reflux, 17 h

2: 99 percent / 36percent conc. HCl, H₃PO₄ / acetic acid / 36 h / 90 - 95 °C

With hydrogenchloride; N,N,N,N,N,N-hexamethylphosphoric triamide; phosphoric acid; iodine; magnesium; copper(I) bromide; In acetic acid;