dimethyl (2'S,2R)-(+)-4-<2-(methoxymethyl)pyrrolidinoimino>-2,4-diphenyl-1,1-butanedicarboxylate

Base Information

Chemical Name:dimethyl (2'S,2R)-(+)-4-<2-(methoxymethyl)pyrrolidinoimino>-2,4-diphenyl-1,1-butanedicarboxylate
CAS No.:109012-78-4
Molecular Formula:C₂₆H₃₂N₂O₅
Molecular Weight:452.55
Hs Code.:

Synonyms:dimethyl (2'S,2R)-(+)-4-<2-(methoxymethyl)pyrrolidinoimino>-2,4-diphenyl-1,1-butanedicarboxylate

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Chemical Property of dimethyl (2'S,2R)-(+)-4-<2-(methoxymethyl)pyrrolidinoimino>-2,4-diphenyl-1,1-butanedicarboxylate

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Technology Process of dimethyl (2'S,2R)-(+)-4-<2-(methoxymethyl)pyrrolidinoimino>-2,4-diphenyl-1,1-butanedicarboxylate

There total 3 articles about dimethyl (2'S,2R)-(+)-4-<2-(methoxymethyl)pyrrolidinoimino>-2,4-diphenyl-1,1-butanedicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 59983-39-0,187035-29-6
(S)-1-amino-2-(methoxymethyl)pyrrolidine

: 109012-78-4
dimethyl (2'S,2R)-(+)-4-<2-(methoxymethyl)pyrrolidinoimino>-2,4-diphenyl-1,1-butanedicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / p-TsOH / benzene / Heating

2: 1) n-BuLi, diisopropylamine / 1) n-hexane, THF, 0 deg C, 2 h, 2) -78 deg C, 2 h, to 0 deg C within 8-12 h

With n-butyllithium; toluene-4-sulfonic acid; diisopropylamine; In benzene;

Reference yield:

: 98-86-2
acetophenone

: 109012-78-4
dimethyl (2'S,2R)-(+)-4-<2-(methoxymethyl)pyrrolidinoimino>-2,4-diphenyl-1,1-butanedicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / p-TsOH / benzene / Heating

2: 1) n-BuLi, diisopropylamine / 1) n-hexane, THF, 0 deg C, 2 h, 2) -78 deg C, 2 h, to 0 deg C within 8-12 h

With n-butyllithium; toluene-4-sulfonic acid; diisopropylamine; In benzene;

Reference yield:

: 6626-84-2
dimethyl 2-benzylidenepropanedioate

: 89393-53-3
(S)-(-)-2-methoxymethyl-1-(1-phenylethylideneamino)pyrrolidine

: dimethyl (2'S,2S)-(+)-4-<2-(methoxymethyl)pyrrolidinoimino>-2,4-diphenyl-1,1-butanedicarboxylate

: 109012-78-4
dimethyl (2'S,2R)-(+)-4-<2-(methoxymethyl)pyrrolidinoimino>-2,4-diphenyl-1,1-butanedicarboxylate

Guidance literature:: With n-butyllithium; diisopropylamine; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1) n-hexane, THF, 0 deg C, 2 h, 2) -78 deg C, 2 h, to 0 deg C within 8-12 h;