2--2-phenylethanenitrile

Base Information

• Chemical Name: 2--2-phenylethanenitrile
• CAS No.: 710307-06-5
• Molecular Formula: C₁₈H₂₀N₂O
• Molecular Weight: 280.37

Synonyms:2--2-phenylethanenitrile

Chemical Property of 2--2-phenylethanenitrile

Chemical Property:

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Technology Process of 2--2-phenylethanenitrile

There total 2 articles about 2--2-phenylethanenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

potassium cyanide (151-50-8) + benzaldehyde (100-52-7) + L-ephedrine hydrochloride → 2--2-phenylethanenitrile (710307-06-5)

Guidance literature:

In water; acetonitrile; for 5h; Ambient temperature;

Reference yield:

potassium cyanide (151-50-8) + (2S,4S,5R)-3,4-dimethyl-2,5-diphenyloxazolidine (89675-44-5) → 2--2-phenylethanenitrile (710307-06-5)

Guidance literature:

With citric acid; In ethanol; water;

DOI:10.1016/j.tetlet.2004.03.092

Reference yield: 94.0%

2--2-phenylethanenitrile (710307-06-5) → (3R,5S,6R)-4,5-dimethyl-3,6-diphenylperhydro-1,4-oxazin-2-one (29843-11-6)

Guidance literature:

With hydrogenchloride; In benzene; at 27 ℃; for 48h;

upstream raw materials:

potassium cyanide

benzaldehyde

(2S,4S,5R)-3,4-dimethyl-2,5-diphenyloxazolidine

Downstream raw materials:

(3R,5S,6R)-4,5-dimethyl-3,6-diphenylperhydro-1,4-oxazin-2-one

(2S,4S,5R)-3,4-dimethyl-2,5-diphenyloxazolidine

[((1S,2R)-2-Chloro-1-methyl-2-phenyl-ethyl)-methyl-amino]-phenyl-acetonitrile

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