(RR)-N,N’ -(1,2-diphenylethane-1,2- diyl)dipicolinamide

Base Information

• Chemical Name: (RR)-N,N’ -(1,2-diphenylethane-1,2- diyl)dipicolinamide
• CAS No.: 230312-36-4
• Molecular Formula: C₂₆H₂₂N₄O₂
• Molecular Weight: 422.486
• Mol file: 230312-36-4.mol

Synonyms:(RR)-N,N’ -(1,2-diphenylethane-1,2- diyl)dipicolinamide

Chemical Property of (RR)-N,N’ -(1,2-diphenylethane-1,2- diyl)dipicolinamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (RR)-N,N’ -(1,2-diphenylethane-1,2- diyl)dipicolinamide

There total 1 articles about (RR)-N,N’ -(1,2-diphenylethane-1,2- diyl)dipicolinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2-Picolinic acid (98-98-6) + (R,R)-1,2-diphenylethylenediamine (35132-20-8) → (RR)-N,N’ -(1,2-diphenylethane-1,2- diyl)dipicolinamide (230312-36-4)

Guidance literature:

2-Picolinic acid; With 1,1'-carbonyldiimidazole; In tetrahydrofuran; at 50 ℃; for 1h;

(R,R)-1,2-diphenylethylenediamine; In tetrahydrofuran; at 20 ℃;

DOI:10.1016/j.jorganchem.2004.06.014

Reference yield:

potassium tetrachloroplatinate(II) (10025-99-7) + (RR)-N,N’ -(1,2-diphenylethane-1,2- diyl)dipicolinamide (230312-36-4) → C26H20N4O2Pt

Guidance literature:

With 18-crown-6 ether; In 2-ethoxy-ethanol; at 135 - 140 ℃; for 24h; Inert atmosphere;

DOI:10.1016/j.cclet.2021.08.104

Reference yield:

zirconium(IV) tert-butoxide + (RR)-N,N’ -(1,2-diphenylethane-1,2- diyl)dipicolinamide (230312-36-4) → [Zr(O(t)Bu)2(1R,2R)-N,N'-bis(2-pyridinecarboxyamido)-1,2-diphenylethane]

Guidance literature:

In benzene; Zr compd. added to a suspn. of ligand at 70°C under Ar, cooled toroom temp. for 5 h;

DOI:10.1016/j.jorganchem.2004.06.014

upstream raw materials:

2-Picolinic acid

(R,R)-1,2-diphenylethylenediamine