4-(aminomethyl)-N,N,N'-trimethylbenzenesulfonimidamide

Base Information

Chemical Name:4-(aminomethyl)-N,N,N'-trimethylbenzenesulfonimidamide
CAS No.:1570084-62-6
Molecular Formula:C₁₀H₁₇N₃OS
Molecular Weight:227.33
Hs Code.:

Synonyms:4-(aminomethyl)-N,N,N'-trimethylbenzenesulfonimidamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(aminomethyl)-N,N,N'-trimethylbenzenesulfonimidamide

Chemical Property:

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Technology Process of 4-(aminomethyl)-N,N,N'-trimethylbenzenesulfonimidamide

There total 7 articles about 4-(aminomethyl)-N,N,N'-trimethylbenzenesulfonimidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1570084-60-4
2-[[4-[S-(dimethylamino)-N-methyl-sulfonimidoyl]phenyl]methyl]isoindoline-1,3-dione

: 1570084-62-6
4-(aminomethyl)-N,N,N'-trimethylbenzenesulfonimidamide

Guidance literature:: With ethylenediamine; In tetrahydrofuran; ethanol; acetonitrile; at 60 ℃; for 6.5h;

Reference yield:

: 2142-01-0
N-benzylphthalimide

: 1570084-62-6
4-(aminomethyl)-N,N,N'-trimethylbenzenesulfonimidamide

Guidance literature:: Multi-step reaction with 7 steps

1.1: chlorosulfonic acid / dichloromethane / 1.5 h / 0 - 20 °C

1.2: 3.5 h / 0 °C / Reflux

1.3: 20 °C

2.1: triphenylphosphine / toluene / 2.5 h / 0 - 20 °C

3.1: triphenylphosphine / N,N-dimethyl-formamide / 2 h / 20 °C

4.1: acetic anhydride; sulfuryl dichloride / dichloromethane / 1 h / -20 °C

5.1: tetrahydrofuran / 2 h / 0 °C

6.1: tert-butylhypochlorite / acetonitrile / 0.25 h / 0 °C

6.2: 0 - 20 °C

7.1: ethylenediamine / ethanol; acetonitrile; tetrahydrofuran / 6.5 h / 60 °C

With chlorosulfonic acid; sulfuryl dichloride; tert-butylhypochlorite; acetic anhydride; ethylenediamine; triphenylphosphine; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile;

Reference yield:

: 1570084-56-8
thioacetic acid 4-(1,3-dioxo-1,3-dihydro-isoindol-2-ylmethyl)-phenyl ester

: 1570084-62-6
4-(aminomethyl)-N,N,N'-trimethylbenzenesulfonimidamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetic anhydride; sulfuryl dichloride / dichloromethane / 1 h / -20 °C

2.1: tetrahydrofuran / 2 h / 0 °C

3.1: tert-butylhypochlorite / acetonitrile / 0.25 h / 0 °C

3.2: 0 - 20 °C

4.1: ethylenediamine / ethanol; acetonitrile; tetrahydrofuran / 6.5 h / 60 °C

With sulfuryl dichloride; tert-butylhypochlorite; acetic anhydride; ethylenediamine; In tetrahydrofuran; ethanol; dichloromethane; acetonitrile;