2-[[4-[S-(dimethylamino)-N-methyl-sulfonimidoyl]phenyl]methyl]isoindoline-1,3-dione

Base Information

Chemical Name:2-[[4-[S-(dimethylamino)-N-methyl-sulfonimidoyl]phenyl]methyl]isoindoline-1,3-dione
CAS No.:1570084-60-4
Molecular Formula:C₁₈H₁₉N₃O₃S
Molecular Weight:357.433
Hs Code.:

Synonyms:2-[[4-[S-(dimethylamino)-N-methyl-sulfonimidoyl]phenyl]methyl]isoindoline-1,3-dione

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Chemical Property of 2-[[4-[S-(dimethylamino)-N-methyl-sulfonimidoyl]phenyl]methyl]isoindoline-1,3-dione

Chemical Property:

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Technology Process of 2-[[4-[S-(dimethylamino)-N-methyl-sulfonimidoyl]phenyl]methyl]isoindoline-1,3-dione

There total 6 articles about 2-[[4-[S-(dimethylamino)-N-methyl-sulfonimidoyl]phenyl]methyl]isoindoline-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1570084-58-0
4-(1,3-dioxo-1,3-dihydro-isoindol-2-ylmethyl)-benzenesulfinic acid methylamide

: 124-40-3
dimethyl amine

: 1570084-60-4
2-[[4-[S-(dimethylamino)-N-methyl-sulfonimidoyl]phenyl]methyl]isoindoline-1,3-dione

Guidance literature:: 4-(1,3-dioxo-1,3-dihydro-isoindol-2-ylmethyl)-benzenesulfinic acid methylamide; With tert-butylhypochlorite; In acetonitrile; at 0 ℃; for 0.25h;

dimethyl amine; In tetrahydrofuran; acetonitrile; at 0 - 20 ℃;

Reference yield:

: 1570084-56-8
thioacetic acid 4-(1,3-dioxo-1,3-dihydro-isoindol-2-ylmethyl)-phenyl ester

: 1570084-60-4
2-[[4-[S-(dimethylamino)-N-methyl-sulfonimidoyl]phenyl]methyl]isoindoline-1,3-dione

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic anhydride; sulfuryl dichloride / dichloromethane / 1 h / -20 °C

2.1: tetrahydrofuran / 2 h / 0 °C

3.1: tert-butylhypochlorite / acetonitrile / 0.25 h / 0 °C

3.2: 0 - 20 °C

With sulfuryl dichloride; tert-butylhypochlorite; acetic anhydride; In tetrahydrofuran; dichloromethane; acetonitrile;

Reference yield:

: 402925-20-6
4-[(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)methyl]benzenesulphonyl chloride

: 1570084-60-4
2-[[4-[S-(dimethylamino)-N-methyl-sulfonimidoyl]phenyl]methyl]isoindoline-1,3-dione

Guidance literature:: Multi-step reaction with 5 steps

1.1: triphenylphosphine / toluene / 2.5 h / 0 - 20 °C

2.1: triphenylphosphine / N,N-dimethyl-formamide / 2 h / 20 °C

3.1: acetic anhydride; sulfuryl dichloride / dichloromethane / 1 h / -20 °C

4.1: tetrahydrofuran / 2 h / 0 °C

5.1: tert-butylhypochlorite / acetonitrile / 0.25 h / 0 °C

5.2: 0 - 20 °C

With sulfuryl dichloride; tert-butylhypochlorite; acetic anhydride; triphenylphosphine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile;