thioacetic acid 4-(1,3-dioxo-1,3-dihydro-isoindol-2-ylmethyl)-phenyl ester

Base Information

Chemical Name:thioacetic acid 4-(1,3-dioxo-1,3-dihydro-isoindol-2-ylmethyl)-phenyl ester
CAS No.:1570084-56-8
Molecular Formula:C₁₇H₁₃NO₃S
Molecular Weight:311.361
Hs Code.:

Synonyms:thioacetic acid 4-(1,3-dioxo-1,3-dihydro-isoindol-2-ylmethyl)-phenyl ester

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Chemical Property of thioacetic acid 4-(1,3-dioxo-1,3-dihydro-isoindol-2-ylmethyl)-phenyl ester

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Technology Process of thioacetic acid 4-(1,3-dioxo-1,3-dihydro-isoindol-2-ylmethyl)-phenyl ester

There total 5 articles about thioacetic acid 4-(1,3-dioxo-1,3-dihydro-isoindol-2-ylmethyl)-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: 7790-94-5
chlorosulfonic acid

: 2142-01-0
N-benzylphthalimide

: 1570084-56-8
thioacetic acid 4-(1,3-dioxo-1,3-dihydro-isoindol-2-ylmethyl)-phenyl ester

Guidance literature:: chlorosulfonic acid; N-benzylphthalimide; In dichloromethane; at 0 - 20 ℃; for 1.5h;

With thionyl chloride; at 0 ℃; for 3.5h; Reflux;

Reference yield:

: C₁₅H₁₁NO₂S

: 108-24-7
acetic anhydride

: 1570084-56-8
thioacetic acid 4-(1,3-dioxo-1,3-dihydro-isoindol-2-ylmethyl)-phenyl ester

Guidance literature:: With triphenylphosphine; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

Reference yield:

: 402925-20-6
4-[(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)methyl]benzenesulphonyl chloride

: 108-24-7
acetic anhydride

: 1570084-56-8
thioacetic acid 4-(1,3-dioxo-1,3-dihydro-isoindol-2-ylmethyl)-phenyl ester

Guidance literature:: 4-[(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)methyl]benzenesulphonyl chloride; With triphenylphosphine; In toluene; at 0 - 20 ℃; for 2.5h;

acetic anhydride; In N,N-dimethyl-formamide; at 20 ℃; for 2h;