4-(1,3-dioxo-1,3-dihydro-isoindol-2-ylmethyl)-benzenesulfinic acid methylamide

Base Information

Chemical Name:4-(1,3-dioxo-1,3-dihydro-isoindol-2-ylmethyl)-benzenesulfinic acid methylamide
CAS No.:1570084-58-0
Molecular Formula:C₁₆H₁₄N₂O₃S
Molecular Weight:314.365
Hs Code.:

Synonyms:4-(1,3-dioxo-1,3-dihydro-isoindol-2-ylmethyl)-benzenesulfinic acid methylamide

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Chemical Property of 4-(1,3-dioxo-1,3-dihydro-isoindol-2-ylmethyl)-benzenesulfinic acid methylamide

Chemical Property:

Purity/Quality:

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Technology Process of 4-(1,3-dioxo-1,3-dihydro-isoindol-2-ylmethyl)-benzenesulfinic acid methylamide

There total 5 articles about 4-(1,3-dioxo-1,3-dihydro-isoindol-2-ylmethyl)-benzenesulfinic acid methylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₅H₁₀ClNO₃S

: 74-89-5
methylamine

: 1570084-58-0
4-(1,3-dioxo-1,3-dihydro-isoindol-2-ylmethyl)-benzenesulfinic acid methylamide

Guidance literature:: In tetrahydrofuran; at 0 ℃; for 2h;

Reference yield:

: 402925-20-6
4-[(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)methyl]benzenesulphonyl chloride

: 1570084-58-0
4-(1,3-dioxo-1,3-dihydro-isoindol-2-ylmethyl)-benzenesulfinic acid methylamide

Guidance literature:: Multi-step reaction with 4 steps

1: triphenylphosphine / toluene / 2.5 h / 0 - 20 °C

2: triphenylphosphine / N,N-dimethyl-formamide / 2 h / 20 °C

3: acetic anhydride; sulfuryl dichloride / dichloromethane / 1 h / -20 °C

4: tetrahydrofuran / 2 h / 0 °C

With sulfuryl dichloride; acetic anhydride; triphenylphosphine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene;

Reference yield:

: 1570084-56-8
thioacetic acid 4-(1,3-dioxo-1,3-dihydro-isoindol-2-ylmethyl)-phenyl ester

: 1570084-58-0
4-(1,3-dioxo-1,3-dihydro-isoindol-2-ylmethyl)-benzenesulfinic acid methylamide

Guidance literature:: Multi-step reaction with 2 steps

1: acetic anhydride; sulfuryl dichloride / dichloromethane / 1 h / -20 °C

2: tetrahydrofuran / 2 h / 0 °C

With sulfuryl dichloride; acetic anhydride; In tetrahydrofuran; dichloromethane;