Technology Process of N-methyl-N-<2-(o-bromophenyl)ethoxy>amine
There total 4 articles about N-methyl-N-<2-(o-bromophenyl)ethoxy>amine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
borane pyridine complex;
In
ethanol; water;
for 3h;
Ambient temperature;
DOI:10.1021/ja00279a058
- Guidance literature:
-
Multi-step reaction with 4 steps
1: lithium aluminum hydride / diethyl ether / 0.67 h / Heating
2: triphenylphosphine, diethyl azodicarboxylate / tetrahydrofuran / 24 h / Ambient temperature
3: 48.4 percent / hydrazine hydrate / ethanol / 2 h / Heating
4: 43.9 percent / pyridine-borane complex / ethanol; H2O / 3 h / Ambient temperature
With
lithium aluminium tetrahydride; borane pyridine complex; hydrazine hydrate; triphenylphosphine; diethylazodicarboxylate;
In
tetrahydrofuran; diethyl ether; ethanol; water;
DOI:10.1021/ja00279a058
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triphenylphosphine, diethyl azodicarboxylate / tetrahydrofuran / 24 h / Ambient temperature
2: 48.4 percent / hydrazine hydrate / ethanol / 2 h / Heating
3: 43.9 percent / pyridine-borane complex / ethanol; H2O / 3 h / Ambient temperature
With
borane pyridine complex; hydrazine hydrate; triphenylphosphine; diethylazodicarboxylate;
In
tetrahydrofuran; ethanol; water;
DOI:10.1021/ja00279a058
