6,7-dimethoxy-2-[2-(2-methoxyphenyl)ethyl]-3,4-dihydroisoquinolinium trifluoroacetate

Base Information

Chemical Name:6,7-dimethoxy-2-[2-(2-methoxyphenyl)ethyl]-3,4-dihydroisoquinolinium trifluoroacetate
CAS No.:1356165-53-1
Molecular Formula:C₂F₃O₂*C₂₀H₂₄NO₃
Molecular Weight:439.431
Hs Code.:

Synonyms:6,7-dimethoxy-2-[2-(2-methoxyphenyl)ethyl]-3,4-dihydroisoquinolinium trifluoroacetate

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Chemical Property of 6,7-dimethoxy-2-[2-(2-methoxyphenyl)ethyl]-3,4-dihydroisoquinolinium trifluoroacetate

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Technology Process of 6,7-dimethoxy-2-[2-(2-methoxyphenyl)ethyl]-3,4-dihydroisoquinolinium trifluoroacetate

There total 4 articles about 6,7-dimethoxy-2-[2-(2-methoxyphenyl)ethyl]-3,4-dihydroisoquinolinium trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 52289-93-7
o-Methoxybenzyl bromide

: 1356165-53-1
6,7-dimethoxy-2-[2-(2-methoxyphenyl)ethyl]-3,4-dihydroisoquinolinium trifluoroacetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium hexamethylsilazane / tetrahydrofuran / 0.08 h / -78 °C / Inert atmosphere

1.2: -78 °C / Inert atmosphere

2.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 20 °C / Inert atmosphere

3.1: dibenzoyl peroxide / water / 2.5 h / 80 °C / Inert atmosphere

With sodium tetrahydroborate; potassium hexamethylsilazane; dibenzoyl peroxide; In tetrahydrofuran; methanol; water;
DOI:10.1002/ejoc.201101183

Reference yield:

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1-(2-methoxybenzyl)-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline

: 76-05-1
trifluoroacetic acid

: 1356165-53-1
6,7-dimethoxy-2-[2-(2-methoxyphenyl)ethyl]-3,4-dihydroisoquinolinium trifluoroacetate

Guidance literature:: With dibenzoyl peroxide; In water; at 80 ℃; for 2.5h; Inert atmosphere;
DOI:10.1002/ejoc.201101183

Reference yield:

: 608141-09-9
1-(2-methoxybenzyl)-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline

: 1356165-53-1
6,7-dimethoxy-2-[2-(2-methoxyphenyl)ethyl]-3,4-dihydroisoquinolinium trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / tetrahydrofuran; methanol / 20 °C / Inert atmosphere

2: dibenzoyl peroxide / water / 2.5 h / 80 °C / Inert atmosphere

With sodium tetrahydroborate; dibenzoyl peroxide; In tetrahydrofuran; methanol; water;
DOI:10.1002/ejoc.201101183