N-(2-(2-(2-(2-hydroxyethoxy)ethoxy)ethoxy)ethyl)-3,4-dithiophenolmaleimide

Base Information

• Chemical Name: N-(2-(2-(2-(2-hydroxyethoxy)ethoxy)ethoxy)ethyl)-3,4-dithiophenolmaleimide
• CAS No.: 1442447-59-7
• Molecular Formula: C₂₄H₂₇NO₆S₂
• Molecular Weight: 489.613
• Mol file: 1442447-59-7.mol

Synonyms:N-(2-(2-(2-(2-hydroxyethoxy)ethoxy)ethoxy)ethyl)-3,4-dithiophenolmaleimide

Chemical Property of N-(2-(2-(2-(2-hydroxyethoxy)ethoxy)ethoxy)ethyl)-3,4-dithiophenolmaleimide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(2-(2-(2-(2-hydroxyethoxy)ethoxy)ethoxy)ethyl)-3,4-dithiophenolmaleimide

There total 3 articles about N-(2-(2-(2-(2-hydroxyethoxy)ethoxy)ethoxy)ethyl)-3,4-dithiophenolmaleimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

N-methoxycarbonyl-3,4-dithiophenoylmaleimide (1442447-50-8) + 11-amino-3,6,9-trioxaundecanol (86770-74-3) → N-(2-(2-(2-(2-hydroxyethoxy)ethoxy)ethoxy)ethyl)-3,4-dithiophenolmaleimide (1442447-59-7)

Guidance literature:

N-methoxycarbonyl-3,4-dithiophenoylmaleimide; 11-amino-3,6,9-trioxaundecanol; In dichloromethane; for 24h;

With silica gel; In dichloromethane;

DOI:10.1016/j.tetlet.2013.04.088

Reference yield:

3,4-bis(phenylsulfanyl)-2,5-dihydro-1H-pyrrole-2,5-dione (32774-53-1) → N-(2-(2-(2-(2-hydroxyethoxy)ethoxy)ethoxy)ethyl)-3,4-dithiophenolmaleimide (1442447-59-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 4-methyl-morpholine / ethyl acetate / 0.5 h / 20 °C

2: dichloromethane / 24 h

With 4-methyl-morpholine; In dichloromethane; ethyl acetate;

DOI:10.1016/j.tetlet.2013.04.088

Reference yield:

thiophenol (108-98-5) → N-(2-(2-(2-(2-hydroxyethoxy)ethoxy)ethoxy)ethyl)-3,4-dithiophenolmaleimide (1442447-59-7)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium acetate / methanol / 0.5 h / 20 °C

2: 4-methyl-morpholine / ethyl acetate / 0.5 h / 20 °C

3: dichloromethane / 24 h

With 4-methyl-morpholine; sodium acetate; In methanol; dichloromethane; ethyl acetate;

DOI:10.1016/j.tetlet.2013.04.088

upstream raw materials:

3,4-bis(phenylsulfanyl)-2,5-dihydro-1H-pyrrole-2,5-dione

N-methoxycarbonyl-3,4-dithiophenoylmaleimide

11-amino-3,6,9-trioxaundecanol

thiophenol