methyl 2-(2-(4-chlorophenyl-sulfonyl)ethylsulfonyl)acetate

Base Information

• Chemical Name: methyl 2-(2-(4-chlorophenyl-sulfonyl)ethylsulfonyl)acetate
• CAS No.: 1377727-89-3
• Molecular Formula: C₁₁H₁₃ClO₆S₂
• Molecular Weight: 340.806
• Mol file: 1377727-89-3.mol

Synonyms:methyl 2-(2-(4-chlorophenyl-sulfonyl)ethylsulfonyl)acetate

Chemical Property of methyl 2-(2-(4-chlorophenyl-sulfonyl)ethylsulfonyl)acetate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of methyl 2-(2-(4-chlorophenyl-sulfonyl)ethylsulfonyl)acetate

There total 1 articles about methyl 2-(2-(4-chlorophenyl-sulfonyl)ethylsulfonyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

methanol (67-56-1) + C10H11ClO6S2 (1374025-04-3) → methyl 2-(2-(4-chlorophenyl-sulfonyl)ethylsulfonyl)acetate (1377727-89-3)

Guidance literature:

With sulfuric acid; Reflux;

DOI:10.1002/jhet.865

Reference yield: 80.0%

methyl 2-(2-(4-chlorophenyl-sulfonyl)ethylsulfonyl)acetate (1377727-89-3) + ethanolamine (141-43-5) → C12H14ClNO5S2 (1390645-72-3)

Guidance literature:

ethanolamine; With n-butyllithium; samarium(III) chloride; In toluene; at 0 ℃; Reflux;

methyl 2-(2-(4-chlorophenyl-sulfonyl)ethylsulfonyl)acetate; In toluene; Reflux;

DOI:10.1002/jhet.865

Reference yield: 72.0%

methyl 2-(2-(4-chlorophenyl-sulfonyl)ethylsulfonyl)acetate (1377727-89-3) + Cysteamine (60-23-1) → C12H14ClNO4S3 (1390645-78-9)

Guidance literature:

Cysteamine; With n-butyllithium; samarium(III) chloride; In toluene; at 0 ℃; Reflux;

methyl 2-(2-(4-chlorophenyl-sulfonyl)ethylsulfonyl)acetate; In toluene; Reflux;

DOI:10.1002/jhet.865

upstream raw materials:

methanol

C₁₀H₁₁ClO₆S₂

Downstream raw materials:

N-(2-hydroxyethyl)-2-(4-chlorophenylsulfonylethylsulfonyl)acetamide

C₁₂H₁₄ClNO₅S₂

S-2-aminoethyl 2-(2-(4-chlorophenylsulfonyl)ethylsulfonyl)ethanethioate

C₁₂H₁₄ClNO₄S₃