(2-(1-(phenylsulfonyl)-1H-indol-3-yl)-1H-imidazol-4-yl)(3,4,5-trimethoxyphenyl)methanone

Base Information

Chemical Name:(2-(1-(phenylsulfonyl)-1H-indol-3-yl)-1H-imidazol-4-yl)(3,4,5-trimethoxyphenyl)methanone
CAS No.:1393085-30-7
Molecular Formula:C₂₇H₂₃N₃O₆S
Molecular Weight:517.562
Hs Code.:

Synonyms:(2-(1-(phenylsulfonyl)-1H-indol-3-yl)-1H-imidazol-4-yl)(3,4,5-trimethoxyphenyl)methanone

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Chemical Property of (2-(1-(phenylsulfonyl)-1H-indol-3-yl)-1H-imidazol-4-yl)(3,4,5-trimethoxyphenyl)methanone

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Technology Process of (2-(1-(phenylsulfonyl)-1H-indol-3-yl)-1H-imidazol-4-yl)(3,4,5-trimethoxyphenyl)methanone

There total 6 articles about (2-(1-(phenylsulfonyl)-1H-indol-3-yl)-1H-imidazol-4-yl)(3,4,5-trimethoxyphenyl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1332881-55-6
(1-(phenylsulfonyl)-2-(1-(phenylsulfonyl)-1H-indol-3-yl)-1H-imidazol-4-yl)(3,4,5-trimethoxyphenyl)methanone

: 1393085-30-7
(2-(1-(phenylsulfonyl)-1H-indol-3-yl)-1H-imidazol-4-yl)(3,4,5-trimethoxyphenyl)methanone

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran;

Reference yield:

: 98-09-9
benzenesulfonyl chloride

: 1393085-30-7
(2-(1-(phenylsulfonyl)-1H-indol-3-yl)-1H-imidazol-4-yl)(3,4,5-trimethoxyphenyl)methanone

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium hydroxide / ethanol; acetone / 0.5 h / 20 °C

2.1: ammonium hydroxide / ethanol; water / 0 - 20 °C

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.33 h / 0 °C

4.1: tert.-butyl lithium / tetrahydrofuran; pentane / 0.17 h / -78 °C

4.2: -78 °C

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran

With ammonium hydroxide; tetrabutyl ammonium fluoride; tert.-butyl lithium; sodium hydride; potassium hydroxide; In tetrahydrofuran; ethanol; water; acetone; mineral oil; pentane;

Reference yield:

: 80360-20-9
1-(phenylsulfonyl)indole-3-carbaldehyde

: 1393085-30-7
(2-(1-(phenylsulfonyl)-1H-indol-3-yl)-1H-imidazol-4-yl)(3,4,5-trimethoxyphenyl)methanone

Guidance literature:: Multi-step reaction with 4 steps

1.1: ammonium hydroxide / ethanol; water / 0 - 20 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.33 h / 0 °C

3.1: tert.-butyl lithium / tetrahydrofuran; pentane / 0.17 h / -78 °C

3.2: -78 °C

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran

With ammonium hydroxide; tetrabutyl ammonium fluoride; tert.-butyl lithium; sodium hydride; In tetrahydrofuran; ethanol; water; mineral oil; pentane;