(1-(phenylsulfonyl)-2-(1-(phenylsulfonyl)-1H-indol-3-yl)-1H-imidazol-4-yl)(3,4,5-trimethoxyphenyl)methanone

Base Information

Chemical Name:(1-(phenylsulfonyl)-2-(1-(phenylsulfonyl)-1H-indol-3-yl)-1H-imidazol-4-yl)(3,4,5-trimethoxyphenyl)methanone
CAS No.:1332881-55-6
Molecular Formula:C₃₃H₂₇N₃O₈S₂
Molecular Weight:657.725
Hs Code.:

Synonyms:(1-(phenylsulfonyl)-2-(1-(phenylsulfonyl)-1H-indol-3-yl)-1H-imidazol-4-yl)(3,4,5-trimethoxyphenyl)methanone

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Chemical Property of (1-(phenylsulfonyl)-2-(1-(phenylsulfonyl)-1H-indol-3-yl)-1H-imidazol-4-yl)(3,4,5-trimethoxyphenyl)methanone

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Technology Process of (1-(phenylsulfonyl)-2-(1-(phenylsulfonyl)-1H-indol-3-yl)-1H-imidazol-4-yl)(3,4,5-trimethoxyphenyl)methanone

There total 3 articles about (1-(phenylsulfonyl)-2-(1-(phenylsulfonyl)-1H-indol-3-yl)-1H-imidazol-4-yl)(3,4,5-trimethoxyphenyl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 1332881-60-3
1-(phenylsulfonyl)-3-(1-(phenylsulfonyl)-1H-imidazol-2-yl)-1H-indole

: 4521-61-3
3,4,5-Trimethoxybenzoyl chloride

: 1332881-55-6
(1-(phenylsulfonyl)-2-(1-(phenylsulfonyl)-1H-indol-3-yl)-1H-imidazol-4-yl)(3,4,5-trimethoxyphenyl)methanone

Guidance literature:: 1-(phenylsulfonyl)-3-(1-(phenylsulfonyl)-1H-imidazol-2-yl)-1H-indole; With tert.-butyl lithium; In tetrahydrofuran; pentane; at -78 ℃; for 0.166667h; Inert atmosphere;

3,4,5-Trimethoxybenzoyl chloride; In tetrahydrofuran; pentane; at -78 ℃;

Reference yield:

: 80360-20-9
1-(phenylsulfonyl)indole-3-carbaldehyde

: 1332881-55-6
(1-(phenylsulfonyl)-2-(1-(phenylsulfonyl)-1H-indol-3-yl)-1H-imidazol-4-yl)(3,4,5-trimethoxyphenyl)methanone

Guidance literature:: Multi-step reaction with 3 steps

1.1: ammonium hydroxide / ethanol; water / 0 - 20 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.33 h / 0 °C

3.1: tert.-butyl lithium / tetrahydrofuran; pentane / 0.17 h / -78 °C

3.2: -78 °C

With ammonium hydroxide; tert.-butyl lithium; sodium hydride; In tetrahydrofuran; ethanol; water; mineral oil; pentane;

Reference yield:

: 98-09-9
benzenesulfonyl chloride

: 1332881-55-6
(1-(phenylsulfonyl)-2-(1-(phenylsulfonyl)-1H-indol-3-yl)-1H-imidazol-4-yl)(3,4,5-trimethoxyphenyl)methanone

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium hydroxide / ethanol; acetone / 0.5 h / 20 °C

2.1: ammonium hydroxide / ethanol; water / 0 - 20 °C

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.33 h / 0 °C

4.1: tert.-butyl lithium / tetrahydrofuran; pentane / 0.17 h / -78 °C

4.2: -78 °C

With ammonium hydroxide; tert.-butyl lithium; sodium hydride; potassium hydroxide; In tetrahydrofuran; ethanol; water; acetone; mineral oil; pentane;