Technology Process of C10H9BrO4
There total 4 articles about C10H9BrO4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C9H6Br3FO2; sodium methylate;
In
methanol;
at 65 ℃;
for 4h;
With
hydrogenchloride;
In
methanol; water;
pH=2;
DOI:10.1016/j.bmcl.2011.12.096
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 0.5 h / 20 °C
2.1: potassium carbonate / N,N-dimethyl-formamide / 0.17 h / 20 °C
2.2: 1 h / 20 °C
3.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 2 h / Inert atmosphere; Reflux
4.1: methanol / 4 h / 65 °C
4.2: pH 2
With
sodium chlorite; N-Bromosuccinimide; 2-methyl-but-2-ene; sodium dihydrogenphosphate dihydrate; potassium carbonate; dibenzoyl peroxide;
In
methanol; tetrachloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1016/j.bmcl.2011.12.096
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 0.17 h / 20 °C
1.2: 1 h / 20 °C
2.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 2 h / Inert atmosphere; Reflux
3.1: methanol / 4 h / 65 °C
3.2: pH 2
With
N-Bromosuccinimide; potassium carbonate; dibenzoyl peroxide;
In
methanol; tetrachloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.12.096
