4-(tert-Butoxycarbonylamino-methyl)-cyclohexanecarboxylic acid 2,2-dimethyl-propionyloxymethyl ester

Base Information

Chemical Name:4-(tert-Butoxycarbonylamino-methyl)-cyclohexanecarboxylic acid 2,2-dimethyl-propionyloxymethyl ester
CAS No.:87589-21-7
Molecular Formula:C₁₉H₃₃NO₆
Molecular Weight:371.474
Hs Code.:

Synonyms:4-(tert-Butoxycarbonylamino-methyl)-cyclohexanecarboxylic acid 2,2-dimethyl-propionyloxymethyl ester

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Chemical Property of 4-(tert-Butoxycarbonylamino-methyl)-cyclohexanecarboxylic acid 2,2-dimethyl-propionyloxymethyl ester

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Technology Process of 4-(tert-Butoxycarbonylamino-methyl)-cyclohexanecarboxylic acid 2,2-dimethyl-propionyloxymethyl ester

There total 3 articles about 4-(tert-Butoxycarbonylamino-methyl)-cyclohexanecarboxylic acid 2,2-dimethyl-propionyloxymethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 87589-21-7
4-(tert-Butoxycarbonylamino-methyl)-cyclohexanecarboxylic acid 2,2-dimethyl-propionyloxymethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / NaOH / H₂O; 2-methyl-propan-2-ol / 18 h / Ambient temperature

2: 1.) tetrabutylammonium hydrogen sulfate (QHSO₄), 2 M aq. NaOH / 2.) trichloroethylene, reflux, 3 h

With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In water; tert-butyl alcohol;
DOI:10.1021/jm00154a004

Reference yield:

: 1197-18-8
trans-4-aminomethyl-cyclohexyl-carboxylic acid

: 87589-21-7
4-(tert-Butoxycarbonylamino-methyl)-cyclohexanecarboxylic acid 2,2-dimethyl-propionyloxymethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / NaOH / H₂O; 2-methyl-propan-2-ol / 18 h / Ambient temperature

2: 1.) tetrabutylammonium hydrogen sulfate (QHSO₄), 2 M aq. NaOH / 2.) trichloroethylene, reflux, 3 h

With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In water; tert-butyl alcohol;
DOI:10.1021/jm00154a004

Reference yield:

: 18997-19-8
Chloromethyl pivalate

: 27687-14-5
trans 4-(tert-butyloxycarbonylamino)methylcyclohexanecarboxylic acid

: 87589-21-7
4-(tert-Butoxycarbonylamino-methyl)-cyclohexanecarboxylic acid 2,2-dimethyl-propionyloxymethyl ester

Guidance literature:: With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; Multistep reaction; 2.) trichloroethylene, reflux, 3 h;
DOI:10.1021/jm00154a004