Technology Process of C30H30N8O2S
There total 13 articles about C30H30N8O2S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
N-ethyl-N,N-diisopropylamine; HATU;
In
N,N-dimethyl-formamide;
at 20 ℃;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1-methyl-pyrrolidin-2-one / 1.58 h / 19 - 28 °C
2: 1,3-bis[(diphenylphosphino)propane]dichloronickel(II) / tetrahydrofuran / 4 h / 19 °C / Inert atmosphere
3: trifluoroacetic acid / 2 h / 65 °C
4: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 20 °C
With
1,3-bis[(diphenylphosphino)propane]dichloronickel(II); N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid;
In
tetrahydrofuran; 1-methyl-pyrrolidin-2-one; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / Reflux
2: potassium carbonate / N,N-dimethyl-formamide / 5 h / 70 °C
3: lithium aluminium tetrahydride / tetrahydrofuran / 5 h / 0 °C
4: thionyl chloride / dichloromethane / 5 h / 20 °C
5: sodium iodide / N,N-dimethyl-formamide / 2 h / 70 °C
6: water; hydrogenchloride / 1,4-dioxane / 90 °C
7: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 20 °C
With
hydrogenchloride; N-Bromosuccinimide; lithium aluminium tetrahydride; thionyl chloride; water; potassium carbonate; N-ethyl-N,N-diisopropylamine; HATU; sodium iodide; dibenzoyl peroxide;
In
tetrahydrofuran; 1,4-dioxane; tetrachloromethane; dichloromethane; N,N-dimethyl-formamide;